Framework Characterization of Mesostructured Carbon CMK-1 by X-Ray Powder Diffraction and Electron Microscopy Научная публикация
Журнал |
The Journal of Physical Chemistry B
ISSN: 1520-6106 , E-ISSN: 1520-5207 |
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Вых. Данные | Год: 2002, Том: 106, Номер: 47, Страницы: 12198-12202 Страниц : 5 DOI: 10.1021/jp0257653 | ||||||
Ключевые слова | Mesoporous materials; Textures; Transmission electron microscopy; X ray powder diffraction | ||||||
Авторы |
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Организации |
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Информация о финансировании (3)
1 | Российский фонд фундаментальных исследований | 02-03-97704 |
2 | International Association for the Promotion of Co-operation with Scientists from the New Independent States of the Former Soviet Union | YSF 2001/2-3 |
3 | International Association for the Promotion of Co-operation with Scientists from the New Independent States of the Former Soviet Union | 01-2283 |
Реферат:
The model of structure and structural transformation of the mesostructured carbon material CMK-1 was established by X-ray powder diffraction (XRD) and transmission electron microscopy (TEM) investigations. The investigations showed that the enantiomeric carbon subframeworks formed within the pores of the MCM-48 mesoporous template used for the material synthesis displaced with respect to one another without significant distortions after the dissolution of the silica wall of the template. The model proposed agrees well with TEM images observed. The XRD structural modeling of CMK-1 done using the continuous density function technique allowed perfect fit of the calculated to the experimental powder diffraction pattern and provided geometric characteristics of the material texture. The structural characteristics obtained agreed fairly well with TEM analysis and with previously reported adsorption data.
Библиографическая ссылка:
Solovyov L.A.
, Zaikovskii V.I.
, Shmakov A.N.
, Belousov O.V.
, Ryoo R.
Framework Characterization of Mesostructured Carbon CMK-1 by X-Ray Powder Diffraction and Electron Microscopy
The Journal of Physical Chemistry B. 2002. V.106. N47. P.12198-12202. DOI: 10.1021/jp0257653 WOS Scopus РИНЦ
Framework Characterization of Mesostructured Carbon CMK-1 by X-Ray Powder Diffraction and Electron Microscopy
The Journal of Physical Chemistry B. 2002. V.106. N47. P.12198-12202. DOI: 10.1021/jp0257653 WOS Scopus РИНЦ
Даты:
Поступила в редакцию: | 15 мар. 2002 г. |
Опубликована в печати: | 1 нояб. 2002 г. |
Идентификаторы БД:
Web of science | WOS:000179543800018 |
Scopus | 2-s2.0-0037191890 |
РИНЦ | 41810728 |
Chemical Abstracts | 2002:837567 |
Chemical Abstracts (print) | 138:43267 |
OpenAlex | W2052893920 |