From In situ to Operando Mode: Experience on Synchrotron X-Ray Defraction at SSTRC
Conference Abstracts
Общее |
Language:
Английский,
Genre:
Conference Abstracts,
Status:
Published,
Source type:
Original
|
Conference |
EuropaCat-XII: 12th European Congress on Catalysis “Catalysis: Balancing the use of fossil and renewable resources”
30 Aug - 4 Sep 2015
,
Казань
|
Source |
EuropaCat XII. Catalysis: Balancing the use of fossil and renewable resources. XII European Congress on Catalysis, Kazan (Russia), 30 August - 4 September, 2015 : Book of Abstracts
Compilation,
Boreskov Institute of Catalysis. Novosibirsk.2015.
2184 c. ISBN 9785906376107.
publication_identifier_short.rinz_identifier_type
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Output data |
Year: 2015,
Pages: 931-932
Pages count
: 2
|
Authors |
Shmakov A.
1,2
,
Vinokurov Z.
1,2
,
Saraev A.
1,2
,
Kaichev V.
1,2
|
Affiliations |
1 |
Boreskov Institute of Catalysis SD RAS, Novosibirsk, Russia
|
2 |
Novosibirsk National Research State University, Novosibirsk, Russia
|
|
Funding (1)
1
|
Russian Science Foundation
|
14-23-00037
|
The report describes results of first experiments on In Situ SR XRD applying parallel analysis of gaseous components of
catalytic reactions at Siberian SR Center. The experiments demonstrated that simple attachment of gas analyzer to reactor cell does not provide Operando mode realization. It is suggested that Operando mode to be performed specific requirements to reactor cell as well as solid to gas components ratio have to be met. Actually, for each particular experimental task or class of tasks an individual reactor cell suitable for definite experimental conditions should be developed and created.