Methodology and Procedure of the Stoichiographic Analysis of Solid Inorganic Substances and Materials
Journal of Analytical Chemistry
, E-ISSN: 1608-3199
Boreskov Institute of Catalysis, Siberian Branch, Russian Academy of Sciences,
pr. Akad. Lavrent’eva 5, Novosibirsk, 630090 Russia
The technical and experimental aspects of creating the conditions of differential dissolution in a flow stoichiographic system are discussed; the scheme of the experimental apparatus, stoichiograph, is presented. The construction, operation conditions of the main units of the stoichiograph, and sample treatment issues are considered. The principles of the creation and optimization of the conditions of the dynamic differential dissolution for the analysis of compounds and materials of the known and unknown phase composition are discussed: the composition of solvents and temperature, and the principles of their variation in time, including those in the processes of stoichiographic titration.