The Thermal Stability of Nanodiamond Surface Groups and Onset of Nanodiamond Graphitization Full article
| Conference |
7th Biennial International Workshop on Fullerenes and Atomic Clusters 27 Jun - 1 Jul 2005 , St. Petersburg |
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| Journal |
Fullerenes Nanotubes and Carbon Nanostructures
ISSN: 1536-383X , E-ISSN: 1536-4046 |
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| Output data | Year: 2006, Volume: 14, Number: 2-3, Pages: 557-564 Pages count : 8 DOI: 10.1080/15363830600666779 | ||
| Tags | Graphitization, Nanodiamond, Surface groups | ||
| Authors |
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| Affiliations |
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Funding (3)
| 1 | Russian Foundation for Basic Research | 05-03-32995 |
| 2 | North Atlantic Treaty Organization | SFP-981051 |
| 3 | Civilian Research and Development Foundation | NO-008-X1 |
Abstract:
The results of study of the surface chemistry of nanodiamonds treated by a mixture of HClO4 and H2SO2 acids are presented. Changes of the composition of surface diamond groups brought up by thermal annealing were monitored by Fourier transformed infrared spectroscopy and temperature‐programmed desorption. The decomposition of oxygen‐containing groups is observed at 300–900°C; CHx groups decompose at 700–1150°C. The process of the annealing of ND was investigated by the X‐ray photoelectron spectroscopy. The clear onset of ND graphitization was observed at temperature of 950°C that is supported by the appearance of sp 2 component in the C1s spectrum. The presence of the N1s peak in spectra of ND is observed in initial and partially graphitized ND annealed up to 1100°C.
Cite:
Butenko Y.V.
, Kuznetsov V.L.
, Paukshtis E.A.
, Stadnichenko A.I.
, Mazov I.N.
, Moseenkov S.I.
, Boronin A.I.
, Kosheev S.V.
The Thermal Stability of Nanodiamond Surface Groups and Onset of Nanodiamond Graphitization
Fullerenes Nanotubes and Carbon Nanostructures. 2006. V.14. N2-3. P.557-564. DOI: 10.1080/15363830600666779 WOS Scopus РИНЦ ANCAN OpenAlex
The Thermal Stability of Nanodiamond Surface Groups and Onset of Nanodiamond Graphitization
Fullerenes Nanotubes and Carbon Nanostructures. 2006. V.14. N2-3. P.557-564. DOI: 10.1080/15363830600666779 WOS Scopus РИНЦ ANCAN OpenAlex
Dates:
| Published print: | Apr 1, 2006 |
| Published online: | Aug 22, 2006 |
Identifiers:
| Web of science: | WOS:000238762900064 |
| Scopus: | 2-s2.0-33745122200 |
| Elibrary: | 13513485 |
| Chemical Abstracts: | 2006:682482 |
| Chemical Abstracts (print): | 146:303157 |
| OpenAlex: | W1987486433 |