Formation of Intermetallic Phases during Mechanical Alloying and Annealing of Cr + 20 wt % Al Mixtures | Sciact - CRIS-system of Boreskov Institute of Catalysis

Formation of Intermetallic Phases during Mechanical Alloying and Annealing of Cr + 20 wt % Al Mixtures Full article

Journal

Inorganic Materials
ISSN: 0020-1685 , E-ISSN: 1608-3172

Output data

Year: 2008, Volume: 44, Number: 6, Pages: 587-591 Pages count : 5 DOI: 10.1134/S0020168508060083

Tags

Differential Scanning Calorimetry; Mechanical Alloy; Mechanochemical Synthesis; Iron Silicide; Differential Dissolution

Authors

Kim J. ¹ , Kwon Y. ¹ , Golubkova G.V. ² , Lomovsky O.I. ² , Dudina D.V. ² , Dovlitova L.S. ³ , Malakhov V.V. ³ , Tikhov S.F. ³ , Usol'tsev V.V. ³ , Sadykov V.A. ³

Affiliations

1	Research Center for Machine Parts and Materials Processing, University of Ulsan, 680-749 Korea
2	Institute of Solid-State Chemistry and Mechanochemistry, Siberian Division, Russian Academy of Sciences, ul. Kutateladze 18, Novosibirsk, 630128 Russia
3	Boreskov Institute of Catalysis, Siberian Division, Russian Academy of Sciences, pr. Akademika Lavrent’eva 5, Novosibirsk, 630090 Russia

Funding (2)

1	Russian Foundation for Basic Research	05-03-32236
2	University of Ulsan

We have studied phase-formation processes in mixtures of Cr and Al (20 wt %) powders in the course of mechanical alloying (MA) and the phase transformations of the samples during subsequent annealing at temperatures of up to 800°ë. The resultant x-ray amorphous intermetallic phases were identified by a differential dissolution method, which allows one to follow the formation of x-ray amorphous and partially crystallized phases. During MA of Cr + Al mixtures, the first to form is x-ray amorphous Cr4Al, which then converts to partially crystallized Cr2Al through reaction with aluminum. The peritectoid decomposition of Cr4Al during heating of the MA samples is accompanied by heat release at 330–350°ë. Heating to 420°ë leads to the formation of Cr5Al8. At 800°ë, Cr5Al8 reacts with Cr to form Cr2Al.

Kim J. , Kwon Y. , Golubkova G.V. , Lomovsky O.I. , Dudina D.V. , Dovlitova L.S. , Malakhov V.V. , Tikhov S.F. , Usol'tsev V.V. , Sadykov V.A.
Formation of Intermetallic Phases during Mechanical Alloying and Annealing of Cr + 20 wt % Al Mixtures
Inorganic Materials. 2008. V.44. N6. P.587-591. DOI: 10.1134/S0020168508060083 WOS Scopus РИНЦ ANCAN OpenAlex

Kim J.S. , Kwon Y.S. , Голубкова Г.В. , Ломовский О.И. , Дудина Д.В. , Довлитова Л.С. , Малахов В.В. , Тихов С.Ф. , Усольцев В.В. , Садыков В.А.
Образование интерметаллидов при механическом сплавлении и отжиге смеси Cr с 20 мас. % Al
Неорганические материалы. 2008. Т.44. №6. С.677-681. РИНЦ

Submitted:	Mar 22, 2007
Accepted:	Oct 30, 2007
Published online:	May 30, 2008
Published print:	Jun 1, 2008

Web of science:	WOS:000256339300008
Scopus:	2-s2.0-44649126026
Elibrary:	13594636
Chemical Abstracts:	2008:671227
Chemical Abstracts (print):	150:102884
OpenAlex:	W2036844132

DB	Citing
Web of science	6
Scopus	7
Elibrary	8
OpenAlex	6