A Gas-Chromatographic Study of the Retention of Reaction Components in the Catalytic Oxidation of b-Picoline to Nicotinic Acid Full article
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Journal of Analytical Chemistry
ISSN: 1061-9348 , E-ISSN: 1608-3199 |
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| Output data | Year: 2008, Volume: 63, Number: 9, Pages: 863-866 Pages count : 4 DOI: 10.1134/S1061934808090116 | ||
| Tags | Nicotinic Acid; Reaction Component; Quinolinic Acid; Terephthalic Acid; Polar Stationary Phasis | ||
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Abstract:
The gas-chromatographic retention of pyridine, β-picoline, 3-pyridinecarbaldehyde, 3-pyridinenitrile,
nicotinic acid, and nicotinamide on polar stationary phases was studied. A scheme was proposed and a
procedure was developed for the determination of the reaction components of the catalytic oxidation of
β-picoline to nicotinic acid on a column (3 m × 3 mm) packed with Chromosorb WAW + 10 wt % FFAP. The
separation time was 28 min. The detection limits were 0.01 and 0.37 ppm for 3-pyridinenitrile and nicotinic
acid, respectively
Cite:
Yakovleva E.Y.
, Belotserkovskaya V.Y.
, Skry'pnik O.V.
A Gas-Chromatographic Study of the Retention of Reaction Components in the Catalytic Oxidation of b-Picoline to Nicotinic Acid
Journal of Analytical Chemistry. 2008. V.63. N9. P.863-866. DOI: 10.1134/S1061934808090116 WOS Scopus РИНЦ ANCAN OpenAlex
A Gas-Chromatographic Study of the Retention of Reaction Components in the Catalytic Oxidation of b-Picoline to Nicotinic Acid
Journal of Analytical Chemistry. 2008. V.63. N9. P.863-866. DOI: 10.1134/S1061934808090116 WOS Scopus РИНЦ ANCAN OpenAlex
Original:
Яковлева Е.Ю.
, Белоцерковская В.Ю.
, Скрыпник О.В.
Исследование удерживания компонентов реакции каталитического окисления β -пиколина в никотиновую кислоту методом газовой хроматографии
Журнал аналитической химии. 2008. Т.63. №9. С.948-952. РИНЦ
Исследование удерживания компонентов реакции каталитического окисления β -пиколина в никотиновую кислоту методом газовой хроматографии
Журнал аналитической химии. 2008. Т.63. №9. С.948-952. РИНЦ
Dates:
| Submitted: | Jun 20, 2007 |
| Accepted: | Nov 20, 2007 |
| Published online: | Aug 20, 2008 |
| Published print: | Sep 1, 2008 |
Identifiers:
| Web of science: | WOS:000258613900011 |
| Scopus: | 2-s2.0-50149094091 |
| Elibrary: | 13583970 |
| Chemical Abstracts: | 2008:1003689 |
| Chemical Abstracts (print): | 150:113444 |
| OpenAlex: | W1991506465 |