A Procedure of ICP-AES Analysis of Silicon Using Microwave Digestion and Preconcentration Full article
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Journal of Analytical Chemistry
ISSN: 1061-9348 , E-ISSN: 1608-3199 |
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| Output data | Year: 2015, Volume: 70, Number: 1, Pages: 28-31 Pages count : 4 DOI: 10.1134/S1061934815010153 | ||||
| Tags | atomic emission spectrochemical analysis, high-purity silicon, inductively coupled plasma, limits of detection, multielemental analysis, preconcentration of impurities | ||||
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Abstract:
A combined procedure has been developed for the analysis of highpurity silicon with preliminary
vaporphase digestion and preconcentration in a microwave oven using inductively coupled plasma atomic
emission spectrometry (ICPAES). Liners for highpressure vessels of microwave oven ensuring the simulta
neous distillation of matrices from 3–4 samples without their contact with the acid solution have been
designed and manufactured. The procedure ensures the determination of up to 30 elements: Ag, Al, Be, Bi,
Ca, Cd, Co, Cr, Cu, Fe, Ga, Hf, In, K, Li, Mn, Mo, Na, Nb, Ni, P, Rb, Sb, Sn, Sr, Ta, V, W, Zn, and Zr with
the limits of detection 10–8 ⎯10–6 wt %.
Cite:
Shaverina A.V.
, Tsygankova A.R.
, Saprykin A.I.
A Procedure of ICP-AES Analysis of Silicon Using Microwave Digestion and Preconcentration
Journal of Analytical Chemistry. 2015. V.70. N1. P.28-31. DOI: 10.1134/S1061934815010153 WOS Scopus РИНЦ ANCAN OpenAlex
A Procedure of ICP-AES Analysis of Silicon Using Microwave Digestion and Preconcentration
Journal of Analytical Chemistry. 2015. V.70. N1. P.28-31. DOI: 10.1134/S1061934815010153 WOS Scopus РИНЦ ANCAN OpenAlex
Original:
Шаверина А.В.
, Цыганкова А.Р.
, Сапрыкин А.И.
Методика ИСП-АЭС анализа кремния с микроволновым разложением и концентрированием
Журнал аналитической химии. 2015. Т.70. №1. С.26-29. DOI: 10.7868/S004445021501017X РИНЦ OpenAlex
Методика ИСП-АЭС анализа кремния с микроволновым разложением и концентрированием
Журнал аналитической химии. 2015. Т.70. №1. С.26-29. DOI: 10.7868/S004445021501017X РИНЦ OpenAlex
Dates:
| Submitted: | Oct 8, 2013 |
| Accepted: | Dec 27, 2013 |
| Published online: | Dec 13, 2014 |
| Published print: | Jan 1, 2015 |
Identifiers:
| Web of science: | WOS:000346239700006 |
| Scopus: | 2-s2.0-85000237252 |
| Elibrary: | 24934182 |
| Chemical Abstracts: | 2014:2091153 |
| Chemical Abstracts (print): | 162:148230 |
| OpenAlex: | W2070855488 |