Chromatographic Properties PLOT Multicapillary Columns Full article
Journal |
Journal of Chromatography A
ISSN: 0021-9673 , E-ISSN: 1873-3778 |
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Output data | Year: 2017, Volume: 1488, Pages: 126-133 Pages count : 8 DOI: 10.1016/j.chroma.2017.01.087 | ||||
Tags | 1-vinylimidazole (VIm), Divinylbenzene (DVB), Gas-solid chromatography, Multicapillary column, PLOT column, Poly-(1-trimethylsilyl-1-propyne) (PTMSP) | ||||
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Abstract:
Multicapillary columns (MCCs) for gas chromatography make it possible to perform high-speed analysis of the mixtures of gaseous and volatile substances at a relatively large amount of the loaded sample. The study was performed using PLOT MCCs for gas-solid chromatography (GSC) with different stationary phases (SP) based on alumina, silica and poly-(1-trimethylsilyl-1-propyne) (PTMSP) polymer as well as porous polymers divinylbenzene-styrene (DVB-St), divinylbenzene-vinylimidazole (DVB-VIm) and divinylbenzene-ethylene glycol dimethacrylate (DVB-EGD). These MCCs have the efficiency of 4000-10000 theoretical plates per meter (TP/m) and at a column length of 25–30 cm can separate within 10–20 s multicomponent mixtures of substances belonging to different classes of chemical compounds. The sample amount not overloading the column is 0.03–1 μg and depends on the features of a porous layer. Examples of separations on some of the studied columns are considered
Cite:
Nikolaeva O.A.
, Patrushev Y.V.
, Sidelnikov V.N.
Chromatographic Properties PLOT Multicapillary Columns
Journal of Chromatography A. 2017. V.1488. P.126-133. DOI: 10.1016/j.chroma.2017.01.087 WOS Scopus РИНЦ ANCAN PMID OpenAlex
Chromatographic Properties PLOT Multicapillary Columns
Journal of Chromatography A. 2017. V.1488. P.126-133. DOI: 10.1016/j.chroma.2017.01.087 WOS Scopus РИНЦ ANCAN PMID OpenAlex
Dates:
Submitted: | Nov 29, 2016 |
Accepted: | Jan 30, 2017 |
Published online: | Feb 1, 2017 |
Published print: | Mar 10, 2017 |
Identifiers:
Web of science: | WOS:000395853700014 |
Scopus: | 2-s2.0-85011339772 |
Elibrary: | 29476454 |
Chemical Abstracts: | 2017:220725 |
Chemical Abstracts (print): | 166:459842 |
PMID: | 28173926 |
OpenAlex: | W2584253675 |