Application of Synchrotron Radiation for in situ XRD Investigation of Zirconium Hydrides Formation at Gas-Phase Hydrogenation Full article
| Conference |
The International Conference "Synchrotron and Free electron laser Radiation: generation and application" 04-07 Jul 2016 , Novosibirsk |
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| Journal |
Physics Procedia
ISSN: 1875-3892 |
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| Output data | Year: 2016, Volume: 84, Pages: 342-348 Pages count : 7 DOI: 10.1016/j.phpro.2016.11.058 | ||||||
| Tags | hydrogen sorption curves, hydrogenation, phase transitions, synchrotron radiation, zirconium alloy | ||||||
| Authors |
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| Affiliations |
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Funding (2)
| 1 | Russian Science Foundation | 14-50-00080 |
| 2 | The Ministry of Education and Science of the Russian Federation | Проект 5-100 |
Abstract:
The zirconium alloy (Zr1%Nb) samples with a micron-thick nickel layer were investigated for hydrogen sorption ability. Hydrogenation was carried out by phase method at temperatures of 350, 450 and 550° C. Hydrogen pressure in chamber was 1 atm. Hydrogen sorption curves were obtained on the automated complex Gas Reaction Controller. In situ X-ray diffraction measurements of the process of hydrogen saturation of samples were carried out at the station “Precision diffractometry» at Siberian Synchrotron and Terahertz Radiation Center of the Budker Institute of Nuclear Physics. Hydrogen absorption rate by Zr1%Nb alloy increases by order of magnitude with increasing temperature. The phase transitions significantly affect the rate of hydrogen absorption at constant temperature. Measurements were performed using SR from the VEPP-3 storage ring.
Cite:
Syrtanov M.S.
, Kudiiarov V.N.
, Kashkarov E.B.
, Shmakov A.N.
, Vinokurov Z.S.
, Babikhina M.N.
, Zolotarev K.V.
Application of Synchrotron Radiation for in situ XRD Investigation of Zirconium Hydrides Formation at Gas-Phase Hydrogenation
Physics Procedia. 2016.
V.84. P.342-348. DOI: 10.1016/j.phpro.2016.11.058
WOS
Scopus
РИНЦ
OpenAlex
AN
Application of Synchrotron Radiation for in situ XRD Investigation of Zirconium Hydrides Formation at Gas-Phase Hydrogenation
Physics Procedia. 2016.
V.84. P.342-348. DOI: 10.1016/j.phpro.2016.11.058
WOS
Scopus
РИНЦ
OpenAlex
AN
Files:
Full text from publisher
Dates:
| Published print: | Jan 1, 2016 |
| Published online: | Dec 12, 2016 |
Identifiers:
| ≡ Web of science: | WOS:000392696400056 |
| ≡ Scopus: | 2-s2.0-85016247483 |
| ≡ Elibrary: | 29482988 |
| ≡ OpenAlex: | W2566285183 |
| ≡ Chemical Abstracts: | 2016:2089583 |