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Synthesis and Сharacterization of 3D Hierarchical Rutile Nanostructures: Effects of Synthesis Temperature and Reagent Concentrations on the Texture and Morphology Full article

Journal Nanotechnologies in Russia
ISSN: 1995-0780 , E-ISSN: 1995-0799
Output data Year: 2017, Volume: 12, Number: 3, Pages: 156-164 Pages count : 9 DOI: 10.1134/S1995078017020045
Tags Nanostructures; Sol-gels
Authors Bessudnova E.V. 1 , Shikina N.V. 1 , Mel’gunov M.S. 1 , Ismagilov Z.R. 1,2
Affiliations
1 Boreskov Institute of Catalysis, Novosibirsk, 630090 Russia
2 Institute of Coal Chemistry and Material Science Federal Research Center of Coal and Coal Chemistry, Kemerovo, 650000 Russia

Funding (1)

1 Federal Agency for Scientific Organizations 0303-2016-0004

Abstract: Rutile nanostructures with a 3D hierarchical structure organization are synthesized via the sol-gel technique using TiCl4 as a titanium precursor and HCl to regulate the acidity. The effects the synthesis conditions—molar ratios of the reagents ([Cl–]/[Ti4+] and [H2O]/[Ti4+]) and temperature—have on the mechanism of formation of the rutile phase are established. We show that the texture and morphology of the rutile nanostructrures depend on the particle packing at all levels of the hierarchical organization and are directly related to the synthesis conditions.
Cite: Bessudnova E.V. , Shikina N.V. , Mel’gunov M.S. , Ismagilov Z.R.
Synthesis and Сharacterization of 3D Hierarchical Rutile Nanostructures: Effects of Synthesis Temperature and Reagent Concentrations on the Texture and Morphology
Nanotechnologies in Russia. 2017. V.12. N3. P.156-164. DOI: 10.1134/S1995078017020045 WOS Scopus РИНЦ AN OpenAlex
Original: Бессуднова Е.В. , Шикина Н.В. , Мельгунов М.С. , Исмагилов З.Р.
Синтез и исследование 3d иерархического нанорутила. Влияние температуры синтеза и концентрации исходных компонентов на текстурные свойства и морфологию
Российские нанотехнологии. 2017. Т.12. №3-4. С.34-42. RSCI РИНЦ
Dates:
Submitted: Aug 10, 2016
Accepted: Dec 13, 2016
Published print: Mar 1, 2017
Published online: Apr 29, 2017
Identifiers:
Web of science: WOS:000410430200005
Scopus: 2-s2.0-85018274494
Elibrary: 31043931
Chemical Abstracts: 2017:684527
OpenAlex: W2609154079
Citing:
DB Citing
Web of science 3
Scopus 1
Elibrary 4
OpenAlex 3
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