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SEM Study of the Surface Morphology and Chemical Composition of the MgAl- and MgGa-Layered Hydroxides in Different Steps of Platinum Catalysts Pt/Mg(Al, Ga)Ox Synthesis Full article

Journal Applied Clay Science
ISSN: 0169-1317 , E-ISSN: 1872-9053
Output data Year: 2018, Volume: 157, Pages: 267-273 Pages count : 7 DOI: 10.1016/j.clay.2018.03.003
Tags Layered double hydroxides Scanning electron microscopy Energy dispersive X-ray spectroscopy Morphology
Authors Stepanova L.N. 1 , Belskaya O.B. 1 , Salanov A.N. 2 , Serkova A.N. 2 , Likholobov V.A. 1
Affiliations
1 Institute of Hydrocarbons Processing SB RAS, Neftezavodskaya St., 54, 644040 Omsk, Russia
2 Boreskov Institute of Catalysis SB RAS, Pr. Acad. Lavrentieva, 5, 630090 Novosibirsk, Russia

Funding (1)

1 Federal Agency for Scientific Organizations V.46.2.4

Abstract: The surface morphology and chemical composition of the MgAl- and MgGa-layered hydroxides as supports precursors were studied by SEM and EDX in all steps of the platinum catalysts Pt/Mg(Ga, Al)Ox synthesis. The study revealed a higher structural stability of Ga-containing samples in comparison with Al-containing analogs, which shows up as their morphological invariability during calcination, activation of layered double hydroxides, and anchoring of the metal complex. A similar Mg/M3+ ratio of metals estimated by both the volumetric method and EDX confirms that a uniform distribution of metals in the support is retained during the catalyst synthesis; this will ensure the specified adsorption and acid-base properties of Pt/MgAlOx and Pt/MgGaOx, which are the promising catalytic systems for dehydrogenation of light and higher alkanes.
Cite: Stepanova L.N. , Belskaya O.B. , Salanov A.N. , Serkova A.N. , Likholobov V.A.
SEM Study of the Surface Morphology and Chemical Composition of the MgAl- and MgGa-Layered Hydroxides in Different Steps of Platinum Catalysts Pt/Mg(Al, Ga)Ox Synthesis
Applied Clay Science. 2018. V.157. P.267-273. DOI: 10.1016/j.clay.2018.03.003 WOS Scopus РИНЦ AN OpenAlex
Dates:
Submitted: Oct 13, 2017
Accepted: Mar 2, 2018
Published online: Mar 9, 2018
Published print: Jun 1, 2018
Identifiers:
Web of science: WOS:000430629500030
Scopus: 2-s2.0-85043356632
Elibrary: 35520621
Chemical Abstracts: 2018:452334
OpenAlex: W2793893510
Citing:
DB Citing
Web of science 16
Scopus 16
Elibrary 15
OpenAlex 17
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