Effect of Pressure on Crystalline L- and DL-Serine: Revisited by a Combined Single-Crystal X-Ray Diffraction at a Laboratory Source and Polarized Raman Spectroscopy Study Full article
| Journal |
Acta Crystallographica Section B. Structural Science (up to 2013)
ISSN: 0108-7681 , E-ISSN: 1600-5740 |
||||||
|---|---|---|---|---|---|---|---|
| Output data | Year: 2012, Volume: 68, Number: 3, Pages: 275-286 Pages count : 12 DOI: 10.1107/S0108768112015960 | ||||||
| Tags | hydrogen bonds; amino acids; high pressure; Raman spectroscopy; single-crystal diffraction at a laboratory source | ||||||
| Authors |
|
||||||
| Affiliations |
|
Abstract:
Information on the effect of pressure on hydrogen bonds, which could be derived from single-crystal X-ray diffraction at a laboratory source and polarized Raman spectroscopy, has been compared. l-Serine and dl-serine were selected for this case study. The role of hydrogen bonds in pressure-induced phase transitions in the first system and in the structural stability of the second one are discussed. Non-monotonic distortion of selected hydrogen bonds in the pressure range below 1-2 GPa, a change in the compression mechanism at 2-3 GPa, and the evidence of formation of bifurcated N - H⋯O hydrogen bonds in dl-serine at 3-4 GPa are considered. © 2012 International Union of Crystallography Printed in Singapore - all rights reserved.
Cite:
Zakharov B.A.
, Kolesov B.A.
, Boldyreva E.V.
Effect of Pressure on Crystalline L- and DL-Serine: Revisited by a Combined Single-Crystal X-Ray Diffraction at a Laboratory Source and Polarized Raman Spectroscopy Study
Acta Crystallographica Section B. Structural Science (up to 2013). 2012. V.68. N3. P.275-286. DOI: 10.1107/S0108768112015960 WOS Scopus РИНЦ ANCAN OpenAlex
Effect of Pressure on Crystalline L- and DL-Serine: Revisited by a Combined Single-Crystal X-Ray Diffraction at a Laboratory Source and Polarized Raman Spectroscopy Study
Acta Crystallographica Section B. Structural Science (up to 2013). 2012. V.68. N3. P.275-286. DOI: 10.1107/S0108768112015960 WOS Scopus РИНЦ ANCAN OpenAlex
Dates:
| Submitted: | Dec 26, 2011 |
| Accepted: | Apr 12, 2012 |
| Published online: | May 17, 2012 |
| Published print: | Jun 1, 2012 |
Identifiers:
| Web of science: | WOS:000304250200007 |
| Scopus: | 2-s2.0-84861385269 |
| Elibrary: | 17986111 |
| Chemical Abstracts: | 2012:718354 |
| Chemical Abstracts (print): | 157:60378 |
| OpenAlex: | W2004827378 |