Reversible Pressure-Induced Disordering in bis(DL-Serinium) Oxalate Dihydrate Научная публикация
| Журнал |
Journal of Molecular Structure
ISSN: 0022-2860 |
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| Вых. Данные | Год: 2014, Том: 1078, Страницы: 151-157 Страниц : 7 DOI: 10.1016/j.molstruc.2014.04.067 | ||||
| Ключевые слова | Amino acid salts, High pressure, Phase transitions, Raman spectroscopy, X-ray diffraction | ||||
| Авторы |
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| Организации |
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Реферат:
We report the study of a reversible phase transition accompanied by pressure-induced disordering in bis(dl-serinium) oxalate dihydrate which was observed at hydrostatic pressures of ∼4 GPa. The disordering manifested itself as a strong diffuse scattering in diffraction patterns and as a similarity of low-wavenumber Raman spectra measured for different polarizations. Several domains were formed, though the single crystals remained intact. On releasing pressure, both the order in the crystal structure and the mono-domain single crystal were restored. Structural strain on increasing pressure prior to the phase transition was studied by single-crystal X-ray diffraction and Raman spectroscopy and compared with that on cooling, as well as with the pressure-induced strain of dl-serine, in which no pressure-induced disordering or structural transitions could be observed.
Библиографическая ссылка:
Zakharov B.A.
, Boldyreva E.V.
Reversible Pressure-Induced Disordering in bis(DL-Serinium) Oxalate Dihydrate
Journal of Molecular Structure. 2014. V.1078. P.151-157. DOI: 10.1016/j.molstruc.2014.04.067 WOS Scopus РИНЦ CAPlusCA OpenAlex
Reversible Pressure-Induced Disordering in bis(DL-Serinium) Oxalate Dihydrate
Journal of Molecular Structure. 2014. V.1078. P.151-157. DOI: 10.1016/j.molstruc.2014.04.067 WOS Scopus РИНЦ CAPlusCA OpenAlex
Даты:
| Поступила в редакцию: | 31 дек. 2013 г. |
| Принята к публикации: | 22 апр. 2014 г. |
| Опубликована online: | 28 апр. 2014 г. |
| Опубликована в печати: | 25 дек. 2014 г. |
Идентификаторы БД:
| Web of science: | WOS:000343845100016 |
| Scopus: | 2-s2.0-84908154383 |
| РИНЦ: | 23995104 |
| Chemical Abstracts: | 2014:1750105 |
| Chemical Abstracts (print): | 161:587478 |
| OpenAlex: | W1968165485 |