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Monolithic Rod Columns for HPLC Based on Divinylbenzene-Styrene Copolymer with 1-Vinylimidazole and 4-Vinylpyridine Full article

Journal Journal of Liquid Chromatography & Related Technologies
ISSN: 1082-6076 , E-ISSN: 1520-572X
Output data Year: 2018, Volume: 41, Number: 8, Pages: 458-466 Pages count : 9 DOI: 10.1080/10826076.2018.1455149
Tags 1-vinylimidazole; 4-vinylpyridine; HPLC; monolithic columns; porous polymers
Authors Patrushev Yuri 1,2 , Yudina Yulia 2 , Sidelnikov Vladimir 1
Affiliations
1 Department of Physicochemical Methods, Boreskov Institute of Catalysis, Novosibirsk, Russia
2 Department of Natural Sciences, Novosibirsk State University, Novosibirsk, Russia

Funding (1)

1 Ministry of Science and Higher Education of the Russian Federation ГЗ-2017-2020

Abstract: Monolithic chromatographic columns for HPLC based on divinylbenzene-styrene both with 1-vinylimidazole and with 4-vinylpyridine are prepared. The monoliths were synthesized in glass tubes with the inner diameter of 2 mm. Texture, hydrodynamic and chromatographic properties of the prepared columns were studied. Linear solvation energy relationships model was applied for the characterization of columns selectivity It is shown that changing the on 1-vinylimidazole or 4-vinylpyridine content in the initial solution allows to change the selectivity of the columns. An examples of small molecules and some proteins separations are presented.
Cite: Patrushev Y. , Yudina Y. , Sidelnikov V.
Monolithic Rod Columns for HPLC Based on Divinylbenzene-Styrene Copolymer with 1-Vinylimidazole and 4-Vinylpyridine
Journal of Liquid Chromatography & Related Technologies. 2018. V.41. N8. P.458-466. DOI: 10.1080/10826076.2018.1455149 WOS Scopus РИНЦ AN OpenAlex
Dates:
Published print: May 9, 2018
Published online: May 24, 2018
Identifiers:
Web of science: WOS:000433145700007
Scopus: 2-s2.0-85047488368
Elibrary: 35484115
Chemical Abstracts: 2018:1017271
OpenAlex: W2804473815
Citing:
DB Citing
Web of science 11
Scopus 12
Elibrary 12
OpenAlex 12
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