Monolithic Rod Columns for HPLC Based on Divinylbenzene-Styrene Copolymer with 1-Vinylimidazole and 4-Vinylpyridine Full article
Journal |
Journal of Liquid Chromatography & Related Technologies
ISSN: 1082-6076 , E-ISSN: 1520-572X |
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Output data | Year: 2018, Volume: 41, Number: 8, Pages: 458-466 Pages count : 9 DOI: 10.1080/10826076.2018.1455149 | ||||
Tags | 1-vinylimidazole; 4-vinylpyridine; HPLC; monolithic columns; porous polymers | ||||
Authors |
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Affiliations |
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Funding (1)
1 | Ministry of Science and Higher Education of the Russian Federation | ГЗ-2017-2020 |
Abstract:
Monolithic chromatographic columns for HPLC based on divinylbenzene-styrene both with 1-vinylimidazole and with 4-vinylpyridine are prepared. The monoliths were synthesized in glass tubes with the inner diameter of 2 mm. Texture, hydrodynamic and chromatographic properties of the prepared columns were studied. Linear solvation energy relationships model was applied for the characterization of columns selectivity It is shown that changing the on 1-vinylimidazole or 4-vinylpyridine content in the initial solution allows to change the selectivity of the columns. An examples of small molecules and some proteins separations are presented.
Cite:
Patrushev Y.
, Yudina Y.
, Sidelnikov V.
Monolithic Rod Columns for HPLC Based on Divinylbenzene-Styrene Copolymer with 1-Vinylimidazole and 4-Vinylpyridine
Journal of Liquid Chromatography & Related Technologies. 2018. V.41. N8. P.458-466. DOI: 10.1080/10826076.2018.1455149 WOS Scopus РИНЦ AN OpenAlex
Monolithic Rod Columns for HPLC Based on Divinylbenzene-Styrene Copolymer with 1-Vinylimidazole and 4-Vinylpyridine
Journal of Liquid Chromatography & Related Technologies. 2018. V.41. N8. P.458-466. DOI: 10.1080/10826076.2018.1455149 WOS Scopus РИНЦ AN OpenAlex
Dates:
Published print: | May 9, 2018 |
Published online: | May 24, 2018 |
Identifiers:
Web of science: | WOS:000433145700007 |
Scopus: | 2-s2.0-85047488368 |
Elibrary: | 35484115 |
Chemical Abstracts: | 2018:1017271 |
OpenAlex: | W2804473815 |