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Production of Nanoscale Crystalline Materials (Si, SiC) by a Highly Efficient Hyperbaric Method Full article

Conference III Всероссийская конференция «Теплофизика и физическая гидродинамика» с элементами школы молодых ученых
10-16 Sep 2018 , Ялта
Journal Journal of Physics: Conference Series
ISSN: 1742-6588 , E-ISSN: 1742-6596
Output data Year: 2018, Volume: 1128, Number: 1, Article number : 012100, Pages count : 6 DOI: 10.1088/1742-6596/1128/1/012100
Tags Ceramic coatings Crystalline materials High resolution transmission electron microscopy Hydrodynamics Pyrolysis Silicon carbide Transmission electron microscopy
Authors Ezdin B S 1 , Kalyada V V 1 , Ischenko A V 1,2 , Zarvin A E 1 , Nikiforov A A 1 , Yatsenko D A 1,2
Affiliations
1 Novosibirsk State University, 1 Pirogova Street, Novosibirsk, 630090, Russia
2 Boreskov Institute of Catalysis SB RAS, 5 Lavrentiev Avenue, Novosibirsk, 630090, Russia

Funding (3)

1 Federal Agency for Scientific Organizations 0303-2016-0002
2 The Ministry of Education and Science of the Russian Federation 3.5920.2017/ИТР
3 The Ministry of Education and Science of the Russian Federation 3.5918.2017/ИТР

Abstract: The method of producing nanopowders of Si and SiC by pyrolysis of a silicon-hydrocarbon mixture by compression in a cyclic process in a flow reactor is proposed and implemented. The obtained powders are characterized by X-ray diffraction and transmission electron microscopy. The new design solutions and use of ceramic coatings obtained by applying microarc oxidation for the piston-cylinder assembly – a compression unit of the reactor - allowed avoiding the use of compression rings and lubricants, achieving a high compression ratio and pressure and temperature in the reactor needed for monosilane pyrolysis. Pyrolysis in the flow reactor is convenient, technological and efficient in terms of its use in the production of high purity nanopowders.
Cite: Ezdin B.S. , Kalyada V.V. , Ischenko A.V. , Zarvin A.E. , Nikiforov A.A. , Yatsenko D.A.
Production of Nanoscale Crystalline Materials (Si, SiC) by a Highly Efficient Hyperbaric Method
Journal of Physics: Conference Series. 2018. V.1128. N1. 012100 :1-6. DOI: 10.1088/1742-6596/1128/1/012100 WOS Scopus РИНЦ AN OpenAlex
Files: Full text from publisher
Dates:
Published online: Dec 6, 2018
Published print: Dec 7, 2018
Identifiers:
Web of science: WOS:000544066400100
Scopus: 2-s2.0-85058637715
Elibrary: 38644189
Chemical Abstracts: 2019:1077005
OpenAlex: W2904430713
Citing: Пока нет цитирований
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