Dimethylsulfoxide as a Media for One-Stage Synthesis of the Fe3O4-Based Ferrofluids with a Controllable Size Distribution Full article
| Journal |
Materials Chemistry and Physics
ISSN: 0254-0584 , E-ISSN: 1879-3312 |
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| Output data | Year: 2019, Volume: 225, Pages: 292-297 Pages count : 6 DOI: 10.1016/j.matchemphys.2019.01.003 | ||||
| Tags | Ferrofluid; Magnetite nanoparticles; One-step synthesis; Superparamagnetic nanoparticles; Ferromagnetic resonance | ||||
| Authors |
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| Affiliations |
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Funding (1)
| 1 | Russian Science Foundation | 17-12-01111 |
Abstract:
The ultrafine (d = 4 nm) magnetite ferrofluid with a narrow nanoparticle size distribution has been synthesized in one stage at room temperature from a solution of iron(II) and (III) chlorides in dimethylsulfoxide (DMSO) with the propylene epoxide admixture. This is the first example of obtaining a stable concentrated ultrafine magnetite/DMSO ferrofluid at room temperature. X-ray diffraction, transmission electron microscopy, ferromagnetic resonance, Mössbauer spectroscopy, and magnetostatic study have been used to elucidate the role of DMSO and the H2O/DMSO ratio in the formation of a stable colloid with a desired nanoparticle size. The initial stages of the magnetite nanoparticles formation have been investigated by the ferromagnetic resonance technique.
Cite:
Kirillov V.L.
, Yakushkin S.S.
, Balaev D.A.
, Dubrovskiy A.A.
, Semenov S.V.
, Knyazev Y.V.
, Bayukov O.A.
, Velikanov D.A.
, Yatsenko D.A.
, Martyanov O.N.
Dimethylsulfoxide as a Media for One-Stage Synthesis of the Fe3O4-Based Ferrofluids with a Controllable Size Distribution
Materials Chemistry and Physics. 2019. V.225. P.292-297. DOI: 10.1016/j.matchemphys.2019.01.003 WOS Scopus РИНЦ AN OpenAlex
Dimethylsulfoxide as a Media for One-Stage Synthesis of the Fe3O4-Based Ferrofluids with a Controllable Size Distribution
Materials Chemistry and Physics. 2019. V.225. P.292-297. DOI: 10.1016/j.matchemphys.2019.01.003 WOS Scopus РИНЦ AN OpenAlex
Dates:
| Submitted: | Aug 21, 2018 |
| Accepted: | Jan 1, 2019 |
| Published online: | Jan 4, 2019 |
| Published print: | Mar 1, 2019 |
Identifiers:
| Web of science: | WOS:000463847900040 |
| Scopus: | 2-s2.0-85060051682 |
| Elibrary: | 38651883 |
| Chemical Abstracts: | 2019:55744 |
| OpenAlex: | W2908414032 |