The In Situ Study of the Fe3O4/DMSO Ferrofluid Synthesis Full article
| Journal |
Applied Magnetic Resonance
ISSN: 0937-9347 , E-ISSN: 1613-7507 |
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| Output data | Year: 2019, Volume: 50, Pages: 1183-1189 Pages count : 7 DOI: 10.1007/s00723-019-01136-6 | ||
| Tags | IRON-OXIDE NANOPARTICLES; MAGNETITE NANOPARTICLES; STABILIZATION; LIQUID | ||
| Authors |
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| Affiliations |
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Funding (2)
| 1 | Russian Foundation for Basic Research | 18-33-00501 |
| 2 | Federal Agency for Scientific Organizations | 0303-2016-0001 |
Abstract:
Electron spin resonance in situ was applied to study the initial stages of ferrofluid formation in combination with the X-ray diffraction, high-resolution transmission electron microscopy and Fourier transform infrared spectroscopy studies data. The ultrafine (d = 4 nm) magnetite in dimethylsulfoxide ferrofluid with a narrow size nanoparticles distribution was obtained in a single step at room temperature by admixing butylene oxide to a solution of iron (II) and (III) chlorides in dimethylsulfoxide. It has been shown that at the first step of the ferrofluid synthesis antiferromagnetically ordered iron containing phase is formed, which can be correlated with iron hydroxides.
Cite:
Yakushkin S.S.
, Kirillov V.L.
, Shalygin A.S.
, Martyanov O.N.
The In Situ Study of the Fe3O4/DMSO Ferrofluid Synthesis
Applied Magnetic Resonance. 2019. V.50. P.1183-1189. DOI: 10.1007/s00723-019-01136-6 WOS Scopus РИНЦ OpenAlex AN
The In Situ Study of the Fe3O4/DMSO Ferrofluid Synthesis
Applied Magnetic Resonance. 2019. V.50. P.1183-1189. DOI: 10.1007/s00723-019-01136-6 WOS Scopus РИНЦ OpenAlex AN
Dates:
| Submitted: | Mar 22, 2019 |
| Accepted: | May 23, 2019 |
| Published online: | Jun 17, 2019 |
| Published print: | Oct 1, 2019 |
Identifiers:
| ≡ Web of science: | WOS:000487007500004 |
| ≡ Scopus: | 2-s2.0-85068033514 |
| ≡ Elibrary: | 41698053 |
| ≡ OpenAlex: | W2950952126 |
| ≡ Chemical Abstracts: | 2019:1185655 |