Synchrotron Radiation Method for Study the Dynamics of Nanoparticle Sizes in Trinitrotoluene During Detonation | Sciact - CRIS-система Института катализа

Synchrotron Radiation Method for Study the Dynamics of Nanoparticle Sizes in Trinitrotoluene During Detonation Научная публикация

Конференция

The International Conference "Synchrotron and Free electron laser Radiation: generation and application"
04-07 июл. 2016 , Novosibirsk

Журнал

Physics Procedia
ISSN: 1875-3892

Вых. Данные

Год: 2016, Том: 84, Страницы: 374-381 Страниц : 8 DOI: 10.1016/j.phpro.2016.11.064

Ключевые слова

Synchrotron radiation, small-angle X-ray scattering, nanodiamond, trinitrotoluene, carbon condensation

Авторы

Rubtsov I.A. ^1,4 , Ten K.A. ^1,4 , Pruuel E.R. ^1,4 , Kashkarov A.O. ^1,4 , Tolochko B.P. ^2,3 , Shechtman L.I. ^2,4 , Zhulanov V.V. ^2,4

Организации

1	Lavrentyev Institute of Hydrodynamics SB RAS
2	Budker Institute of Nuclear Physics SB RAS
3	Institute of Solid State Chemistry and Mechanochemistry SB RAS
4	Novosibirsk State University

This work presents the results of experiments using synchrotron radiation from the VEPP-4M accelerator complex at Budker Institute of Nuclear Physics. Dynamic of small-angle X-ray scattering of synchrotron radiation was implemented on the synchrotron radiation beamline 8-b. Here given beam parameters and described elements of the station and detector system. The distance from the axis of the explosive charge to the detector was 3432 mm. The strip size of the detector DIMEX was 0.1 mm. Thus, a single channel of the detector DIMEX in these experiments corresponded to the scattering angle 2θ: 1 detector channel = 0.02914 mrad. The SAXS measurement technique on this station enables detection of nanoparticles ranging in size from 2 nm to 200 nm with exposure time 73 ps for one frame. It is possible to record 100 frames with interval 100 ns. In this work used TNT with 30 mm in diameter and 55 mm in length. Ultra fine diamonds of 2 nm size was detected behind the detonation front, after that the average size of particles increases up to 5–6 nm during few microseconds.

Rubtsov I.A. , Ten K.A. , Pruuel E.R. , Kashkarov A.O. , Tolochko B.P. , Shechtman L.I. , Zhulanov V.V.
Synchrotron Radiation Method for Study the Dynamics of Nanoparticle Sizes in Trinitrotoluene During Detonation

Physics Procedia. 2016. V.84. P.374-381. DOI: 10.1016/j.phpro.2016.11.064 WOS Scopus РИНЦ CAPlus OpenAlex

Полный текст от издателя

Опубликована online:

12 дек. 2016 г.

Web of science:	WOS:000392696400061
Scopus:	2-s2.0-85016241437
РИНЦ:	29500783
Chemical Abstracts:	2016:2089603
OpenAlex:	W2561445698

БД	Цитирований
Web of science	4
Scopus	6
OpenAlex	10