Sciact
  • EN
  • RU

Study of Supported Metal Catalysts by the Methods of the Small-Angle Scattering of Neutrons and X-rays Full article

Journal Journal of Surface Investigation: X-Ray, Synchrotron and Neutron Techniques
ISSN: 1027-4510 , E-ISSN: 1819-7094
Output data Year: 2021, Volume: 15, Number: 5, Pages: 903-907 Pages count : 5 DOI: 10.1134/s1027451021050074
Tags small-angle neutron scattering, small-angle X-ray scattering, contrast variation, deposited metal catalysts, particle size distributions
Authors Larichev Yu.V. 1,2 , Ivankov O.I. 3,4,5
Affiliations
1 Boreskov Institute of Catalysis, Siberian Branch, Russian Academy of Sciences, Novosibirsk, 630090 Russia
2 Novosibirsk State University, Novosibirsk, 630090 Russia
3 Joint Institute for Nuclear Research, Dubna, Moscow oblast, 141980 Russia
4 Institute for Safety Problems of Nuclear Power Plants, National Academy of Sciences of Ukraine, Kyiv, 07270 Ukraine
5 Moscow Institute of Physics and Technology, Dolgoprudny, Moscow oblast, 141701 Russia

Funding (1)

1 Federal Agency for Scientific Organizations 0303-2016-0002

Abstract: The possibility of analyzing deposited metal catalysts by small-angle neutron scattering through contrast variation based on the use of H2O/D2O mixtures is shown. The use of the contrasting technique makes it possible to selectively obtain the size distribution of metal particles in a wide range of sizes. The reliability of the obtained size distributions of metal particles is confirmed by the additional data of transmission electron microscopy and X-ray diffractometry. Variation in the contrast in small-angle neutron scattering with the use of deuterated liquids is shown to have greater possibilities with respect to the structural analysis of deposited catalysts in comparison with small-angle X-ray scattering.
Cite: Larichev Y.V. , Ivankov O.I.
Study of Supported Metal Catalysts by the Methods of the Small-Angle Scattering of Neutrons and X-rays
Journal of Surface Investigation: X-Ray, Synchrotron and Neutron Techniques. 2021. V.15. N5. P.903-907. DOI: 10.1134/s1027451021050074 WOS Scopus РИНЦ AN OpenAlex
Original: Ларичев Ю.В. , Иваньков О.И.
Исследование нанесенных металлических катализаторов методами малоуглового рассеяния нейтронов и рентгеновских лучей
Поверхность. Рентгеновские, синхротронные и нейтронные исследования. 2021. №9. С.13-18. DOI: 10.31857/s1028096021090077 РИНЦ OpenAlex
Dates:
Submitted: Jan 25, 2020
Accepted: Mar 25, 2021
Published print: Sep 1, 2021
Published online: Oct 19, 2021
Identifiers:
Web of science: WOS:000708904800005
Scopus: 2-s2.0-85117576109
Elibrary: 47516103
Chemical Abstracts: 2021:2283439
OpenAlex: W3207529085
Citing:
DB Citing
Scopus 1
Web of science 1
Elibrary 1
OpenAlex 1
Altmetrics: