New Solvent-Free Melting-Assisted Preparation of Energetic Compound of Nickel with Imidazole for Combustion Synthesis of Ni-Based Materials Full article
| Journal |
Nanomaterials
, E-ISSN: 2079-4991 |
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| Output data | Year: 2021, Volume: 11, Number: 12, Article number : 3332, Pages count : 20 DOI: 10.3390/nano11123332 | ||
| Tags | nickel complex; imidazole; solvent-free melt synthesis; energetic compound; combustion; Ni; NiO | ||
| Authors |
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| Affiliations |
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Funding (1)
| 1 | Ministry of Science and Higher Education of the Russian Federation | 075-15-2020-781 |
Abstract:
In this work two approaches to the synthesis of energetic complex compound Ni(Im)6(NO3)2 from imidazole and nicklel (II) nitrate were applied: a traditional synthesis from solution and a solvent-free melting-assisted method. According to infrared spectroscopy, X-ray diffraction, elemental and thermal analysis data, it was shown that the solvent-free melt synthesis is a faster, simpler and environmentally friendly method of Ni(Im)6(NO3)2 preparation. The results show that this compound is a promising precursor for the production of nanocrystalline Ni-NiO materials by air-assisted combustion method. The combustion of this complex together with inorganic supports makes it possible to synthesize supported nickel catalysts for different catalytic processes
Cite:
Komova O.V.
, Mukha S.A.
, Ozerova A.M.
, Bulavchenko O.A.
, Pochtar A.A.
, Ishchenko A.V.
, Odegova G.V.
, Suknev A.P.
, Netskina O.V.
New Solvent-Free Melting-Assisted Preparation of Energetic Compound of Nickel with Imidazole for Combustion Synthesis of Ni-Based Materials
Nanomaterials. 2021. V.11. N12. 3332 :1-20. DOI: 10.3390/nano11123332 WOS Scopus РИНЦ AN PMID OpenAlex
New Solvent-Free Melting-Assisted Preparation of Energetic Compound of Nickel with Imidazole for Combustion Synthesis of Ni-Based Materials
Nanomaterials. 2021. V.11. N12. 3332 :1-20. DOI: 10.3390/nano11123332 WOS Scopus РИНЦ AN PMID OpenAlex
Dates:
| Submitted: | Nov 16, 2021 |
| Accepted: | Dec 5, 2021 |
| Published online: | Dec 8, 2021 |
| Published print: | Dec 21, 2021 |
Identifiers:
| Web of science: | WOS:000736198300001 |
| Scopus: | 2-s2.0-85120708705 |
| Elibrary: | 47539144 |
| Chemical Abstracts: | 2022:92077 |
| PMID: | 34947681 |
| OpenAlex: | W4200055622 |