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Synthesis of Barium Aluminate of Disk-Shaped Morphology Using the Product of Centrifugal Thermal Activation of Gibbsite Full article

Journal Russian Journal of Applied Chemistry
ISSN: 1070-4272 , E-ISSN: 1608-3296
Output data Year: 2022, Volume: 95, Number: 4, Pages: 512–518 Pages count : 8 DOI: 10.1134/S1070427222040061
Tags gibbsite, product of centrifugal thermal activation of gibbsite, barium aluminate
Authors Zhuzhgov A.V. 1 , Kruglyakov V.Yu. 1 , Suprun E.A. 1 , Isupova L.A. 1
Affiliations
1 Boreskov Institute of Catalysis, Siberian Branch, Russian Academy of Sciences, Novosibirsk, 630090 Russia

Funding (1)

1 Ministry of Science and Higher Education of the Russian Federation 0239-2021-0004

Abstract: Barium aluminate BaAl2O4 of spinel structure was prepared by hydrothermal treatment at 150°С of a suspension of a gibbsite thermal activation product in an aqueous barium nitrate solution, followed by heat treatment of the precursors obtained. The product composition was studied by X-ray diffraction, thermal, microscopic, adsorption, and chemical analysis methods. Heat treatment of the hydrothermal reaction products at 850°С leads to the formation of single-phase barium aluminate BaAl2O4 with the specific surface area of ~50 m2 g–1 in the form of disk-shaped porous particles forming aggregates. The surface of BaAl2O4 particles is enriched in barium cations, which are relatively uniformly distributed over particles. The procedure allows reduction of the amount of the starting reactants and of the number of preparation steps, and also minimization or complete exclusion of the wash water formation.
Cite: Zhuzhgov A.V. , Kruglyakov V.Y. , Suprun E.A. , Isupova L.A.
Synthesis of Barium Aluminate of Disk-Shaped Morphology Using the Product of Centrifugal Thermal Activation of Gibbsite
Russian Journal of Applied Chemistry. 2022. V.95. N4. P.512–518. DOI: 10.1134/S1070427222040061 WOS Scopus РИНЦ AN OpenAlex
Original: Жужгов А.В. , Кругляков В.Ю. , Супрун Е.А. , Исупова Л.А.
Синтез алюмината бария дискообразной морфологии с использованием продукта центробежно-термической активации гиббсита
Журнал прикладной химии. 2022. Т.95. №4. С.450-457. DOI: 10.31857/S0044461822040053 РИНЦ
Dates:
Submitted: Jan 8, 2022
Published print: Apr 1, 2022
Accepted: May 26, 2022
Published online: Sep 16, 2022
Identifiers:
Web of science: WOS:000854592900006
Scopus: 2-s2.0-85138163420
Elibrary: 50305689
Chemical Abstracts: 2022:2424079
OpenAlex: W4296210850
Citing:
DB Citing
Web of science 3
Scopus 3
Elibrary 7
OpenAlex 3
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