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Extended Possibilities of Analysis for Supported Metal Catalysts and Nanocomposites by Dynamic Light Scattering Научная публикация

Журнал Kinetics and Catalysis
ISSN: 0023-1584 , E-ISSN: 1608-3210
Вых. Данные Год: 2022, Том: 63, Номер: 5, Страницы: 599-605 Страниц : 7 DOI: 10.1134/S002315842205007X
Ключевые слова dynamic light scattering, supported metal catalysts, nanocomposites, sols, nanoparticles
Авторы Larichev Yu.V. 1,2
Организации
1 Boreskov Institute of Catalysis, Siberian Branch, Russian Academy of Sciences, Novosibirsk, 630090 Russia
2 Novosibirsk State University, Novosibirsk, 630090 Russia

Информация о финансировании (1)

1 Министерство науки и высшего образования Российской Федерации (с 15 мая 2018) 0239-2021-0003

Реферат: This study is a continuation of the work on the use of dynamic light scattering (DLS) for the analysis of active component particle sizes in supported catalysts. It was shown that the proposed STS (from solid to sol) approach is also applicable to supported catalysts based on sparingly soluble supports and nanocomposites. It was found that partial dissolution or destruction of a support with the formation of solution containing the desired nanoparticles is sufficient for effective DLS analysis. It was found that, under certain conditions, the effect of secondary aggregation of nanoparticles in solution can be observed in the course of catalyst dissolution, and this effect can prevent correct measurements. A method was proposed to avoid the secondary aggregation of particles in the course of the selective dissolution of a support. A good agreement between the results obtained by the new (DLS) method and traditional (TEM and XRD) methods was demonstrated.
Библиографическая ссылка: Larichev Y.V.
Extended Possibilities of Analysis for Supported Metal Catalysts and Nanocomposites by Dynamic Light Scattering
Kinetics and Catalysis. 2022. V.63. N5. P.599-605. DOI: 10.1134/S002315842205007X WOS Scopus РИНЦ CAPlus OpenAlex
Оригинальная: Ларичев Ю.В.
Расширенные возможности анализа нанесенных металлических катализаторов и нанокомпозитов методом динамического рассеяния света
Кинетика и катализ. 2022. Т.63. №5. С.676-683. DOI: 10.31857/S0453881122050082 РИНЦ OpenAlex
Даты:
Поступила в редакцию: 27 дек. 2021 г.
Принята к публикации: 16 апр. 2022 г.
Опубликована online: 23 сент. 2022 г.
Опубликована в печати: 1 окт. 2022 г.
Идентификаторы БД:
Web of science: WOS:000856975300016
Scopus: 2-s2.0-85138612245
РИНЦ: 50421313
Chemical Abstracts: 2022:2471916
OpenAlex: W4297004350
Цитирование в БД:
БД Цитирований
Scopus 2
Web of science 2
РИНЦ 2
OpenAlex 2
Альметрики: