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Experience of Using DLS to Study the Particle Sizes of Active Component in the Catalysts Based on the Oxide and Non-Oxide Supports Научная публикация

Журнал Inorganics
, E-ISSN: 2304-6740
Вых. Данные Год: 2022, Том: 10, Номер: 12, Номер статьи : 248, Страниц : 12 DOI: 10.3390/inorganics10120248
Ключевые слова DLS; STS; particle sizes; supported metal catalysts; porous oxide supports; carbon; polymers; selective dissolution; sols
Авторы Larichev Yurii V. 1,2
Организации
1 Boreskov Institute of Catalysis, Siberian Branch of the Russian Academy of Sciences, Prospekt Akademika Lavrentieva 5, Novosibirsk 630090, Russia
2 Department of Physics, Novosibirsk State University, 1 Pirogov Street, Novosibirsk 630090, Russia

Информация о финансировании (2)

1 Министерство науки и высшего образования Российской Федерации (с 15 мая 2018) FSUS-2020-0029
2 Министерство науки и высшего образования Российской Федерации (с 15 мая 2018) 0239-2021-0003

Реферат: The present study reports the use of the dynamic light scattering (DLS) method to analyze metal nanoparticle sizes in supported catalysts (as a model system for different metal-oxide nanocomposites, ceramics, etc.). The selective dissolution of matrices has been used to transform solids to sols for DLS analysis. DLS/STS (from solid to sol) technique was tested on a wide number of different sets of supported metal catalysts (Pt, Pd, Ru metals and Al2O3, SiO2, TiO2, C3N4, carbon and polymers as supports). The transmission electron microscopy and X-ray diffraction (TEM/XRD) results for the initial supported catalysts and the DLS results for the sols prepared from them showed good agreement with each other. Moreover, it has been shown that this approach can identify the minor contamination of catalysts by large particles or aggregates which are difficult to detect by TEM/XRD.
Библиографическая ссылка: Larichev Y.V.
Experience of Using DLS to Study the Particle Sizes of Active Component in the Catalysts Based on the Oxide and Non-Oxide Supports
Inorganics. 2022. V.10. N12. 248 :1-12. DOI: 10.3390/inorganics10120248 WOS Scopus РИНЦ CAPlus OpenAlex
Даты:
Поступила в редакцию: 14 нояб. 2022 г.
Принята к публикации: 3 дек. 2022 г.
Опубликована online: 8 дек. 2022 г.
Идентификаторы БД:
Web of science: WOS:000901031900001
Scopus: 2-s2.0-85144692703
РИНЦ: 50742588
Chemical Abstracts: 2023:62965
OpenAlex: W4311858766
Цитирование в БД:
БД Цитирований
Scopus 3
РИНЦ 3
OpenAlex 3
Web of science 3
Альметрики: