Synthesis of Boron-Doped Carbon Nanomaterial Научная публикация
| Журнал |
Materials
ISSN: 1996-1944 |
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| Вых. Данные | Год: 2023, Том: 16, Номер: 5, Номер статьи : 1986, Страниц : 11 DOI: 10.3390/ma16051986 | ||
| Ключевые слова | synthesis; graphene; doping; boron | ||
| Авторы |
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| Организации |
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Информация о финансировании (1)
| 1 | Министерство науки и высшего образования Российской Федерации (с 15 мая 2018) | 0239-2021-0010 |
Реферат:
A new method for the synthesis of boron-doped carbon nanomaterial (B-carbon nanomaterial) has been developed. First, graphene was synthesized using the template method. Magnesium oxide was used as the template that was dissolved with hydrochloric acid after the graphene deposition on its surface. The specific surface area of the synthesized graphene was equal to 1300 m2/g. The suggested method includes the graphene synthesis via the template method, followed by the deposition of an additional graphene layer doped with boron in an autoclave at 650 C, using a mixture of phenylboronic acid, acetone, and ethanol. After this carbonization procedure, the mass of the graphene sample increased by 70%. The properties of B-carbon nanomaterial were studied using X-ray photoelectron spectroscopy (XPS), high-resolution transmission electron microscopy (HRTEM), Raman spectroscopy, and adsorption-desorption techniques. The deposition of an additional graphene layer doped with boron led to an increase of the graphene layer thickness from 2–4 to 3–8 monolayers, and a decrease of the specific surface area from 1300 to 800 m2/g. The boron concentration in B-carbon nanomaterial determined by different physical methods was about 4 wt.%.
Библиографическая ссылка:
Chesnokov V.V.
, Prosvirin I.P.
, Gerasimov E.Y.
, Chichkan A.S.
Synthesis of Boron-Doped Carbon Nanomaterial
Materials. 2023. V.16. N5. 1986 :1-11. DOI: 10.3390/ma16051986 WOS Scopus РИНЦ CAPlus PMID OpenAlex
Synthesis of Boron-Doped Carbon Nanomaterial
Materials. 2023. V.16. N5. 1986 :1-11. DOI: 10.3390/ma16051986 WOS Scopus РИНЦ CAPlus PMID OpenAlex
Даты:
| Поступила в редакцию: | 28 окт. 2022 г. |
| Принята к публикации: | 25 февр. 2023 г. |
| Опубликована online: | 28 февр. 2023 г. |
| Опубликована в печати: | 1 мар. 2023 г. |
Идентификаторы БД:
| Web of science: | WOS:000947607300001 |
| Scopus: | 2-s2.0-85149823007 |
| РИНЦ: | 54019905 |
| Chemical Abstracts: | 2023:517678 |
| PMID (PubMed): | 36903101 |
| OpenAlex: | W4322630919 |