A Comprehensive Study on in situ Synthesis of a Magnetic Nanocomposite of Magnetite and Reduced Graphene Oxide and Its Effectiveness at Removing Arsenic from Water Научная публикация
Журнал |
Nano-Structures and Nano-Objects
, E-ISSN: 2352-507X |
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Вых. Данные | Год: 2023, Том: 36, Номер статьи : 101028, Страниц : 18 DOI: 10.1016/j.nanoso.2023.101028 | ||||||||||||||
Ключевые слова | Nanocomposite; Magnetite nanoparticle; Reduced graphene oxide; Adsorption capacity; Water purification; Pollution removal | ||||||||||||||
Авторы |
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Организации |
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Информация о финансировании (4)
1 | Министерство науки и высшего образования Российской Федерации (с 15 мая 2018) | 075-15-2021-588 |
2 | Российский научный фонд | 22-13-20043 (122032900065-0) |
3 | Российский научный фонд | 20-63-47096 (АААА-А20-120052690025-2) |
4 | Министерство науки и высшего образования Российской Федерации (с 15 мая 2018) | 075-15-2021-677 |
Реферат:
In this study, the in situ synthesis of Fe3O4 nanoparticles on the surface of two-dimensional rGO nanosheets was performed. Fe3O4/rGO nanocomposites with a different degree of rGO reduction were obtained using various mass ratios between Fe3O4 and rGO, and different synthesis times. A comprehensive analysis of the morphology, microstructure, magnetic properties and the reduction degree of the synthesized rGO and Fe3O4/rGO nanocomposites was performed. The synthesis conditions were established for the preparation of a Fe3O4/rGO nanocomposite with the highest degree of rGO reduction and Fe3O4 phase purity. An increase in crystallite size and average particle size with the increase in the Fe3O4:rGO mass ratio (from 1:1 to 6:1) was revealed. For the first time, a saturation point for the amount of phase-pure Fe3O4 nanoparticles on the rGO surface was determined, as was a specific ratio of magnetite to rGO at which saturation occurred. Examination of the adsorption isotherms and kinetics indicated that the magnetic Fe3O4/rGO nanocomposite can serve as an effective adsorbent for arsenic ion (As3+) removal from water, with an excellent removal capacity of 14 mg g−1. In addition, the adsorption rate of the Fe3O4/rGO nanocomposite enabled 81% uptake within 1 min, which is superior to the literature data.
Библиографическая ссылка:
Pryadko A.
, Mukhortova Y.R.
, Botvin V.V.
, Grubova I.Y.
, Galstenkova M.R.
, Wagner D.V.
, Gerasimov E.Y.
, Sukhinina E.V.
, Pershina A.G.
, Kholkin A.L.
, Surmeneva M.A.
, Surmenev R.A.
A Comprehensive Study on in situ Synthesis of a Magnetic Nanocomposite of Magnetite and Reduced Graphene Oxide and Its Effectiveness at Removing Arsenic from Water
Nano-Structures and Nano-Objects. 2023. V.36. 101028 :1-18. DOI: 10.1016/j.nanoso.2023.101028 Scopus РИНЦ CAPlusCA OpenAlex
A Comprehensive Study on in situ Synthesis of a Magnetic Nanocomposite of Magnetite and Reduced Graphene Oxide and Its Effectiveness at Removing Arsenic from Water
Nano-Structures and Nano-Objects. 2023. V.36. 101028 :1-18. DOI: 10.1016/j.nanoso.2023.101028 Scopus РИНЦ CAPlusCA OpenAlex
Даты:
Поступила в редакцию: | 13 мая 2023 г. |
Принята к публикации: | 2 авг. 2023 г. |
Опубликована online: | 26 авг. 2023 г. |
Опубликована в печати: | 23 окт. 2023 г. |
Идентификаторы БД:
Scopus: | 2-s2.0-85168811344 |
РИНЦ: | 55990756 |
Chemical Abstracts: | 2023:1861799 |
Chemical Abstracts (print): | 184:123655 |
OpenAlex: | W4386197258 |