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In Situ X-ray Diffraction as a Basic Tool to Study Oxide and Metal Oxide Catalysts Обзор

Журнал Catalysts
ISSN: 2073-4344
Вых. Данные Год: 2023, Том: 13, Номер: 11, Номер статьи : 1421, Страниц : 34 DOI: 10.3390/catal13111421
Ключевые слова in situ XRD; operando XRD; catalyst; oxide; metal
Авторы Bulavchenko Olga A. 1,2 , Vinokurov Zakhar S. 1,3
Организации
1 Boreskov Institute of Catalysis SB RAS, Lavrentiev Ave. 5, 630090 Novosibirsk, Russia
2 Department of Physics, Novosibirsk State University, Pirogova, 2, 630090 Novosibirsk, Russia
3 Synchrotron Radiation Facility SKIF, Boreskov Institute of Catalysis SB RAS, Morskoy 2, 630090 Novosibirsk, Russia

Информация о финансировании (1)

1 Министерство науки и высшего образования Российской Федерации (с 15 мая 2018) 075-15-2022-263

Реферат: X-ray diffraction (XRD) is a standard technique that is widely applied in heterogeneous catalysis to determine phase composition, atomic structure, and size of crystallites. This review is focused on the application of in situ XRD for studying the catalysts during their “lifetime” (under synthesis, activation, operation, and deactivation conditions), limiting the objects of research to oxide and metal oxide catalysts. Also included is a brief overview of modern techniques and instruments and the latest works illustrating different aspects of this technique in catalyst research. The main conclusion is that the field of heterogeneous catalysis research would benefit substantially from the application of in situ XRD for the structural, phase, and morphological characterization of solid catalysts. Even more useful information can be obtained if XRD is combined with other techniques that are more sensitive at length scales different from that of XRD.
Библиографическая ссылка: Bulavchenko O.A. , Vinokurov Z.S.
In Situ X-ray Diffraction as a Basic Tool to Study Oxide and Metal Oxide Catalysts
Catalysts. 2023. V.13. N11. 1421 :1-34. DOI: 10.3390/catal13111421 WOS Scopus РИНЦ OpenAlex CAPlus СКИФ ID
Даты:
Поступила в редакцию: 26 сент. 2023 г.
Принята к публикации: 1 нояб. 2023 г.
Опубликована в печати: 7 нояб. 2023 г.
Опубликована online: 7 нояб. 2023 г.
Идентификаторы БД:
≡ Web of science: WOS:001108178700001
≡ Scopus: 2-s2.0-85178278741
≡ РИНЦ: 55920844
≡ OpenAlex: W4388465473
≡ Chemical Abstracts: 2023:2493115
≡ СКИФ ID: 1375
Цитирование в БД:
≡ OpenAlex 23 Сбор данных от 22.02.2026
≡ Scopus 21 Сбор данных от 22.02.2026
≡ Web of science 20 Сбор данных от 20.02.2026
≡ РИНЦ 8 Сбор данных от 22.02.2026
Альметрики: