Nano-Sized SnO2: Planar Defects or Particle Shape Anisotropy? Full article
| Journal |
Nano-Structures and Nano-Objects
, E-ISSN: 2352-507X |
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| Output data | Year: 2024, Volume: 40, Article number : 101398, Pages count : 6 DOI: 10.1016/j.nanoso.2024.101398 | ||||
| Tags | Cassiterite; Powder X-ray diffraction; Planar defects; Anisotropic particle shape; Structure modeling | ||||
| Authors |
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| Affiliations |
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Funding (1)
| 1 |
Russian Science Foundation Правительство Новосибирской области |
23-23-10086 |
Abstract:
Structure and morphology of nano-sized particles of tin(IV) oxide obtained by oxidative thermolysis of tin(II) oxalate SnC2O4 were studied by powder X-ray diffraction and transmission electron microscopy. The X-ray diffraction pattern corresponds to cassiterite SnO2; however, a strong broadening and a decrease in height of 110 peak are observed. Based on transmission electron microscopy data, it was assumed that planar defects are present in the SnO2 structure. Such defects are observed in nsutite γ-MnO2, the structure of which is disordered and represents an intergrowth of pyrolusite β-MnO2 and ramsdellite R-MnO2 structures. For the first time, a quantitative assessment of such defects in the SnO2 structure was carried out by calculating X-ray diffraction patterns based on statistical models of 1D disordered nanocrystals.
Cite:
Yatsenko D.A.
, Cherepanova S.V.
, Sinitsa N.A.
, Gerasimov E.Y.
, Sidelnikov A.A.
, Matvienko A.A.
Nano-Sized SnO2: Planar Defects or Particle Shape Anisotropy?
Nano-Structures and Nano-Objects. 2024. V.40. 101398 :1-6. DOI: 10.1016/j.nanoso.2024.101398 Scopus РИНЦ AN OpenAlex
Nano-Sized SnO2: Planar Defects or Particle Shape Anisotropy?
Nano-Structures and Nano-Objects. 2024. V.40. 101398 :1-6. DOI: 10.1016/j.nanoso.2024.101398 Scopus РИНЦ AN OpenAlex
Dates:
| Submitted: | Jul 12, 2024 |
| Accepted: | Oct 25, 2024 |
| Published online: | Nov 2, 2024 |
| Published print: | Dec 1, 2024 |
Identifiers:
| Scopus: | 2-s2.0-85207750223 |
| Elibrary: | 75990204 |
| Chemical Abstracts: | 2024:2443083 |
| OpenAlex: | W4404004506 |
Citing:
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