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Portable High Precision Small/Wide Angle X-Ray Scattering Diffractometer Full article

Conference 7th International Conference on Synchrotron Radiation Instrumentation
25-25 Aug 2000 , Berlin
Journal Nuclear Instruments and Methods in Physics Research Section A
ISSN: 0168-9002
Output data Year: 2001, Volume: 467-468, Number: 2, Pages: 1092-1096 Pages count : 5 DOI: 10.1016/S0168-9002(01)00565-4
Tags Data acquisition, Data analysis, Diffractometer, SAXS, Synchrotron radiation
Authors Gaponov Y.A. 1,2 , Dementʹev E.A. 2 , Kochubey D.I. 3 , Tolochko B.P. 1
Affiliations
1 Institute of Solid State Chemistry, Kutateladze, 18, Novosibirsk 630128, Russia
2 Budker Institute of Nuclear Physics, Lavrentyeva, 11, Novosibirsk 630090, Russia
3 Boreskov Institute of Catalysis, Lavrentyeva, 5, Novosibirsk 630090, Russia

Funding (1)

1 Russian Foundation for Basic Research 99-03-32834

Abstract: The portable high precision small/wide angle X-ray scattering diffractometer (modified Bonze–Hart optical scheme) was designed and developed for the investigation of structure rearrangement during liquid state–solid state transformations (with reaction time of 10 h or more) for the investigation of the process of solid state phase formation. The FEM detectors are used as monitor and detector. The double crystal Si111 analyzer (with changeable relative angle of the second crystal) is used as analyzer. All controlling are designed in CAMAC. The diffractometer is controlled by a Sun SPARCStation with SVIC/VCC modules under a Solaris 2.4 operating system, and allows one to obtain the SAXS curves with accuracies (on s-vector for photon energy 8 keV) of about δs∼0.002 nm−1, smin∼0.005 nm−1 (scattering centers with the size of about 200–500 nm may be observed) and smax∼50 nm−1 (scattering angle is about 80°).
Cite: Gaponov Y.A. , Dementʹev E.A. , Kochubey D.I. , Tolochko B.P.
Portable High Precision Small/Wide Angle X-Ray Scattering Diffractometer
Nuclear Instruments and Methods in Physics Research Section A. 2001. V.467-468. N2. P.1092-1096. DOI: 10.1016/S0168-9002(01)00565-4 WOS Scopus РИНЦ ANCAN OpenAlex
Dates:
Published print: Jul 21, 2001
Published online: Aug 7, 2001
Identifiers:
Web of science: WOS:000171012800064
Scopus: 2-s2.0-21844434266
Elibrary: 13364487
Chemical Abstracts: 2001:591493
Chemical Abstracts (print): 135:364196
OpenAlex: W2050925728
Citing:
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Scopus 1
Elibrary 1
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