Variable-Temperature and Variable-Pressure Studies of Small-Molecule Organic Crystals | Sciact - CRIS-system of Boreskov Institute of Catalysis

Variable-Temperature and Variable-Pressure Studies of Small-Molecule Organic Crystals Full article

Journal

Arkivoc
ISSN: 1551-7004 , E-ISSN: 1551-7012

Output data

Year: 2004, Volume: 2004, Number: 12, Pages: 128-155 Pages count : 28 DOI: 10.3998/ark.5550190.0005.c10

Tags

Amino acids, High pressure, Hydrogen bonds, Phase transitions, Polymorphs

Authors

Boldyreva Elena V. ^1,2 , Drebushchak Tatyana N. ^1,2 , Shakhtshneider Tatyana P. ^1,2 , Sowa Heidrun ³ , Ahsbahs Hans ³ , Goryainov Sergei V. ^1,4 , Ivashevskaya Svetlana N. ^1,5 , Kolesnik Evgeniya N. ^1,2 , Drebushchak Valeri A. ^1,4 , Burgina Elena B. ^1,6

Affiliations

1	REC-008 “Molecular Design and Ecologically Safe Technologies”, Novosibirsk State University, Pirogova 2, Novosibirsk 630090 Russia
2	Institute of Solid State Chemistry SB RAS, Novosibirsk, Russia
3	Philipps-Universitaet Marburg, Hans-Meerwein Strasse, D-35032 Marburg/Lahn, Germany
4	Institute of Mineralogy and Petrography SB RAS, Novosibirsk, Russia
5	Institute of Geology Karelian Scientific Center RAS, Petrozavodsk, Russia
6	Boreskov Institute of Catalysis SB RAS, Novosibirsk, Russia

Several examples of the comparative variable-temperature and variable-pressure studies of the small-molecule organic crystals are discussed. Selected systems represent the crystals with nonspherical flexible molecules / molecular fragments and with different types of intermolecular interactions, ranging from van der Waals interactions to hydrogen bonds of various types (OH...O, NH...OH, NH...O=C). A special attention is payed to the studies of solid drugs (polymorphs of paracetamol), amino acids (polymorphs of glycine, L-serine, D,L-serine), and dipeptides (glycilglycine and glycilglycine hydrate) by structural, spectroscopic and calorimetric techniques. The anisotropy of structural distortion within the range of stability of the same phase, as well as the phase transitions induced by changes in temperature or pressure are discussed.

Boldyreva E.V. , Drebushchak T.N. , Shakhtshneider T.P. , Sowa H. , Ahsbahs H. , Goryainov S.V. , Ivashevskaya S.N. , Kolesnik E.N. , Drebushchak V.A. , Burgina E.B.
Variable-Temperature and Variable-Pressure Studies of Small-Molecule Organic Crystals

Arkivoc. 2004. V.2004. N12. P.128-155. DOI: 10.3998/ark.5550190.0005.c10 WOS Scopus РИНЦ OpenAlex

Full text from publisher

Submitted:	Nov 9, 2004
Accepted:	Feb 21, 2005
Published online:	Mar 2, 2005

Web of science:	WOS:000227495900010
Scopus:	2-s2.0-17844369435
Elibrary:	13487246
OpenAlex:	W2518120118

DB	Citing
Web of science	48
Scopus	43
Elibrary	40
OpenAlex	17