From In situ to Operando Mode: Experience on Synchrotron X-Ray Defraction at SSTRC - Conference attendances | Sciact - CRIS-system of Boreskov Institute of Catalysis

From In situ to Operando Mode: Experience on Synchrotron X-Ray Defraction at SSTRC Conference attendances

Language

Английский

Participant type

Стендовый

Conference

EuropaCat-XII: 12th European Congress on Catalysis “Catalysis: Balancing the use of fossil and renewable resources”
30 Aug - 4 Sep 2015 , Казань

Authors

Shmakov Alexander Nikolaevich ^1,2 , Vinokurov Zakhar ^1,2 , Saraev Andrey Aleksandrovich ^1,2 , Kaichev Vasily Vasilievich ^1,2

Affiliations

1	Boreskov Institute of Catalysis SB RAS
2	Novosibirsk National Research University

The report describes results of first experiments on In Situ SR XRD applying parallel analysis of gaseous components of catalytic reactions at Siberian SR Center. The experiments demonstrated that simple attachment of gas analyzer to reactor cell does not provide Operando mode realization. It is suggested that Operando mode to be performed specific requirements to reactor cell as well as solid to gas components ratio have to be met. Actually, for each particular experimental task or class of tasks an individual reactor cell suitable for definite experimental conditions should be developed and created.

Shmakov A.N. , Vinokurov Z. , Saraev A.A. , Kaichev V.V.
From In situ to Operando Mode: Experience on Synchrotron X-Ray Defraction at SSTRC
EuropaCat-XII: 12th European Congress on Catalysis “Catalysis: Balancing the use of fossil and renewable resources” 30 Aug - 4 Sep 2015