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EXAFS and X-Ray RED Study of Polymetalcarbosylanes Full article

Общее Language: Английский, Genre: Full article,
Status: Published, Source type: Original
Conference XII национальная конференция по использованию синхротронного излучения
13-18 Jul 1998 , Новосибирск
Journal Nuclear Instruments and Methods in Physics Research Section A
ISSN: 0168-9002
Output data Year: 2000, Volume: 448, Number: 1-2, Pages: 314-317 Pages count : 4 DOI: 10.1016/S0168-9002(99)00717-2
Authors Kriventsov V.V. 1 , Zyuzin D.A. 1 , Bogdanov S.V. 1 , Moroz E.M. 1 , Gubin S.P. 2 , Tsirlin A.M. 3 , Popova N.A. 3
Affiliations
1 Boreskov Institute of Catalysis, SB RAS, Pr. Lavrentieva, 5, 630090 Novosibirsk, Russia
2 Kurnakov Institute of General and Inorganic Chemistry, RAS, Moscow, Russia
3 State Scientific Center of Russian Federation State Scientific-Research Institute of Chemistry and Technology of Organoelement Compounds, Moscow, Russia

Funding (1)

1 International Association for the Promotion of Co-operation with Scientists from the New Independent States of the Former Soviet Union 96-1410

Abstract: Using EXAES and X-ray RED methods the phase composition of polycarbosylanes containing zirconium has been investigated. It has been demonstrated that metal complex decomposes with introduction into polycarbosylane and formation of metal nanoparticles with the size not exceeding 2 nm and modification of the matrix structure occur. Interaction of the introduced metal with matrix occurs during calcination of sample at 1373–1473 K in nitrogen with forming of zirconium silicide.
Cite: Kriventsov V.V. , Zyuzin D.A. , Bogdanov S.V. , Moroz E.M. , Gubin S.P. , Tsirlin A.M. , Popova N.A.
EXAFS and X-Ray RED Study of Polymetalcarbosylanes
Nuclear Instruments and Methods in Physics Research Section A. 2000. V.448. N1-2. P.314-317. DOI: 10.1016/S0168-9002(99)00717-2 publication_identifier_short.wos_identifier_type publication_identifier_short.scopus_identifier_type publication_identifier_short.rinz_identifier_type
Dates:
Published print: Jun 21, 2000
Published online: Jun 22, 2000
Identifiers:
publication_identifier.wos_identifier_type WOS:000088282500064
publication_identifier.scopus_identifier_type 2-s2.0-0034205291
publication_identifier.rinz_identifier_type 13340105
publication_identifier.accession_number_identifier_type 2000:434638
publication_identifier.chemical_accession_number_identifier_type 133:228205
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