From In situ to Operando Mode: Experience on Synchrotron X-Ray Defraction at SSTRC
The report describes results of first experiments on In Situ SR XRD applying parallel analysis of gaseous components of
catalytic reactions at Siberian SR Center. The experiments demonstrated that simple attachment of gas analyzer to reactor cell does not provide Operando mode realization. It is suggested that Operando mode to be performed specific requirements to reactor cell as well as solid to gas components ratio have to be met. Actually, for each particular experimental task or class of tasks an individual reactor cell suitable for definite experimental conditions should be developed and created.