Preparative Procedure for the Synthesis of 4-Allyloxypyridine-2,6-dicarboxylic Acid | Sciact - CRIS-system of Boreskov Institute of Catalysis

Preparative Procedure for the Synthesis of 4-Allyloxypyridine-2,6-dicarboxylic Acid Full article

Journal

Russian Journal of Organic Chemistry
ISSN: 1070-4280 , E-ISSN: 1608-3393

Output data

Year: 2007, Volume: 43, Number: 1, Pages: 156-157 Pages count : 2 DOI: 10.1134/S107042800701023X

Tags

Dicarboxylic Acid; Dicarboxylate; Diallyl; Aqueous Sodium Hydroxide; Anhydrous Magnesium Sulfate

Authors

Prikhodʹko S.A. ^1,2 , Oleinik I.I. ¹ , Oleinik I.V. ¹ , Ivanchev S.S. ³ , Tolstikov G.A. ¹

Affiliations

1	Vorozhtsov Novosibirsk Institute of Organic Chemistry, Siberian Division, Russian Academy of Sciences, pr. Akademika Lavrent’eva 9, Novosibirsk, 630090 Russia
2	Novosibirsk State University, Novosibirsk, Russia
3	St. Petersburg Division, Boreskov Institute of Catalysis, Siberian Division, Russian Academy of Sciences, St. Petersburg, Russia

Funding (1)

Siberian Branch of the Russian Academy of Sciences

150

The authors describe the preparative procedure for the synthesis of 4-allyloxypyridine-2,6-dicarboxylic acid. The acid 4-allyloxypyridine-2,6-dicarboxylic acid is used as starting compound in the synthesis of 4-allyloxy-2,6-diacetylpyridine. The authors found that acid can be synthesized in two steps and that its yield can be raised to 89% by carrying out alkylation of anhydrous dicarboxylic acid with allyl bromide in the presence of anhydrous potassium carbonate in a mixture of acetone.

Prikhodʹko S.A. , Oleinik I.I. , Oleinik I.V. , Ivanchev S.S. , Tolstikov G.A.
Preparative Procedure for the Synthesis of 4-Allyloxypyridine-2,6-dicarboxylic Acid
Russian Journal of Organic Chemistry. 2007. V.43. N1. P.156-157. DOI: 10.1134/S107042800701023X WOS Scopus РИНЦ ANCAN OpenAlex

Приходько С.А. , Олейник И.И. , Олейник И.В. , Иванчев С.С. , Толстиков Г.А.
Препаративный метод получения 4-аллилокси-2,6-пиридиндикарбоновой кислоты
Журнал органической химии. 2007. Т.43. №1. С.150-151. РИНЦ

Submitted:	Sep 15, 2006
Published print:	Jan 1, 2007

Web of science:	WOS:000244318900023
Scopus:	2-s2.0-33847298082
Elibrary:	13550268
Chemical Abstracts:	2007:171153
Chemical Abstracts (print):	148:239001
OpenAlex:	W2952447261

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