Specific Features of Polyol Synthesis of Silver Nanoparticles with the Use of Solid Carboxylates as Precursors Научная публикация
| Журнал |
Colloid Journal of the Russian Academy of Sciences: Kolloidnyi Zhurnal
ISSN: 1061-933X , E-ISSN: 1608-3067 |
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| Вых. Данные | Год: 2016, Том: 78, Номер: 4, Страницы: 515-524 Страниц : 10 DOI: 10.1134/S1061933X16040189 | ||||
| Ключевые слова | Carboxylation; Ethylene; Ethylene glycol; Mass spectrometry; Metal nanoparticles; Nanoparticles; Organic solvents; Polyols; Salts; Synthesis (chemical); X ray diffraction | ||||
| Авторы |
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| Организации |
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Информация о финансировании (1)
| 1 | Российский научный фонд | 15-13-00113 |
Реферат:
Electron microscopy, Xray diffraction, and chromatography⎯mass spectrometry have been
employed to investigate the reduction of solid silver caprylate in ethylene glycol with the formation of silver
nanoparticles. The structural characteristics of silver nanoparticles have been studied as depending on the
conditions of their synthesis, including temperature, reduction time, and silver salt concentration. It has been
found that, in the studied range of parameters under the conditions, when solid silver caprylate is dispersed
in ethylene glycol, the characteristics of resulting nanoparticles are almost independent of the synthesis tem
perature. This peculiarity is related to the fact that the formation and growth of nanoparticles occur on the
surface of silver salt crystals and are accompanied by gradual dissolution thereof. In this system, ethylene gly
col plays the roles of a reductant and a solvent for liquid reaction products.
Библиографическая ссылка:
Titkov A.I.
, Gerasimov E.Y.
, Shashkov M.V.
, Logutenko O.A.
, Bulina N.V.
, Yukhin Y.M.
, Lyakhov N.Z.
Specific Features of Polyol Synthesis of Silver Nanoparticles with the Use of Solid Carboxylates as Precursors
Colloid Journal of the Russian Academy of Sciences: Kolloidnyi Zhurnal. 2016. V.78. N4. P.515-524. DOI: 10.1134/S1061933X16040189 WOS Scopus РИНЦ CAPlus OpenAlex
Specific Features of Polyol Synthesis of Silver Nanoparticles with the Use of Solid Carboxylates as Precursors
Colloid Journal of the Russian Academy of Sciences: Kolloidnyi Zhurnal. 2016. V.78. N4. P.515-524. DOI: 10.1134/S1061933X16040189 WOS Scopus РИНЦ CAPlus OpenAlex
Оригинальная:
Титков А.И.
, Герасимов Е.Ю.
, Шашков М.В.
, Логутенко О.А.
, Булина Н.В.
, Юхин Ю.М.
, Ляхов Н.З.
Особенности полиольного синтеза наночастиц серебра с использованием твердых карбоксилатов в качестве прекурсоров
Коллоидный журнал. 2016. Т.78. №4. С.490-500. DOI: 10.7868/S0023291216040182 РИНЦ OpenAlex
Особенности полиольного синтеза наночастиц серебра с использованием твердых карбоксилатов в качестве прекурсоров
Коллоидный журнал. 2016. Т.78. №4. С.490-500. DOI: 10.7868/S0023291216040182 РИНЦ OpenAlex
Даты:
| Поступила в редакцию: | 30 нояб. 2015 г. |
| Опубликована в печати: | 1 июл. 2016 г. |
| Опубликована online: | 20 июл. 2016 г. |
Идентификаторы БД:
| Web of science: | WOS:000380227500013 |
| Scopus: | 2-s2.0-84978764808 |
| РИНЦ: | 27076142 |
| Chemical Abstracts: | 2016:1192789 |
| OpenAlex: | W2494511726 |