Sciact
  • EN
  • RU

ICP-AES Techniques of Silicon, Germanium, and Their Oxides Full article

Journal Inorganic Materials
ISSN: 0020-1685 , E-ISSN: 1608-3172
Output data Year: 2016, Volume: 52, Number: 14, Pages: 1431-1438 Pages count : 8 DOI: 10.1134/S0020168516140077
Tags atomic emission spectral analysis, determination of impurities, germanium, germanium oxide (IV), inductively coupled plasma, LODs, matrix effect, silicon, silicon oxide (IV)
Authors Khomichenko N.N. 1,2 , Shaverina A.V. 1 , Tsygankova A.R. 1,2 , Saprykin A.I. 1,2
Affiliations
1 Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences, Novosibirsk, Russia
2 Novosibirsk National Research State University, Novosibirsk, Russia

Abstract: The techniques of atomic emission spectrometry with inductively coupled plasma (ICP-AES) for quantitative determination impuritiesi in silicon, germanium, and their dioxides are developed. Analytical lines for siliconmatrix (29 trace elements) and germanium-matrix (42 trace elements) are selected. Matrix interferences caused by the presence of silicon and germanium in the solutions are studied. The optimal concentrations of matrix are determined. LODs for trace elements are in the range from n × 10–7 to n × 10–5 wt %; RSD < 20%. The accuracy of the results is confirmed by the method of “introduced–found.” The developed techniques are express, simple, and can determine a broad range of trace elements.
Cite: Khomichenko N.N. , Shaverina A.V. , Tsygankova A.R. , Saprykin A.I.
ICP-AES Techniques of Silicon, Germanium, and Their Oxides
Inorganic Materials. 2016. V.52. N14. P.1431-1438. DOI: 10.1134/S0020168516140077 WOS Scopus РИНЦ AN OpenAlex
Original: Хомиченко Н.Н. , Шаверина А.В. , Цыганкова А.Р. , Сапрыкин А.И.
Разработка ИСП-АЭС методик анализа кремния, германия и их оксидов
Заводская лаборатория. Диагностика материалов. 2015. Т.81. №6. С.10-15. RSCI РИНЦ
Dates:
Submitted: Mar 24, 2015
Published print: Dec 1, 2016
Published online: Feb 10, 2017
Identifiers:
Web of science: WOS:000394432700007
Scopus: 2-s2.0-85011827162
Elibrary: 29477131
Chemical Abstracts: 2017:244341
OpenAlex: W2587398790
Citing:
DB Citing
Web of science 5
Scopus 4
OpenAlex 4
Altmetrics: