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Size-Controlled Reverse Microemulsion Synthesis of Ni and Co Metal Nanoparticles Full article

Conference Advanced Materials: Synthesis, Processing and Properties of Nanostructures – 2016 : The Russia-Japan conference
30 Oct - 3 Nov 2016 , Novosibirsk
Journal Materials Today: Proceedings
ISSN: 2214-7853
Output data Year: 2017, Volume: 4, Number: 11, Pages: 11385-11391 Pages count : 7 DOI: 10.1016/j.matpr.2017.09.014
Tags Co, Nanoparticles, Ni, Reverse microemulsion, Synthesis, TEM, UV-Vis
Authors Simakova Irina L. 1,2 , Simonov Mikhail N. 1,2 , Demidova Yuliya S. 1,2 , Murzin Dmitry Yu. 3
Affiliations
1 Boreskov Institute of Catalysis, pr. Ak. Lavrentieva 5, 630090, Novosibirsk, Russia
2 Novosibirsk State University, Pirogova 2, 630090, Novosibirsk, Russia
3 Åbo Akademi University, FI-20500, Turku/Åbo, Finland

Funding (1)

1 European Commission 310490 FP7-NMP-2012-SMALL-6 SUSFUELCAT

Abstract: Microemulsion synthesis of Ni and Co metal nanoparticles with controllable size has been studied in detail to allow replacing expensive metals (Pt and Re) in promising aqueous phase reforming of bio-derivatives. Reduction of nickel or cobalt chloride and nitrate aqueous solutions with N2H4 alkaline solution in the presence of cationic cetyltrimethyl bromide or anionic sodium dodecylsulphosuccinate surfactants provided formation of series of Ni and Co nanoparticles with mean sizes from 2.6 to 3.3 nm and from 1.0 to 5.4 nm, respectively. TEM, XRD, UV-Vis spectroscopy and XPS were applied to determine Ni and Co nanocluster sizes, composition and electronic state.
Cite: Simakova I.L. , Simonov M.N. , Demidova Y.S. , Murzin D.Y.
Size-Controlled Reverse Microemulsion Synthesis of Ni and Co Metal Nanoparticles
Materials Today: Proceedings. 2017. V.4. N11. P.11385-11391. DOI: 10.1016/j.matpr.2017.09.014 WOS Scopus РИНЦ AN OpenAlex
Dates:
Published print: Jan 1, 2017
Published online: Oct 25, 2017
Identifiers:
Web of science: WOS:000416569400014
Scopus: 2-s2.0-85032028659
Elibrary: 31127348
Chemical Abstracts: 2019:1810408
OpenAlex: W2766436766
Citing:
DB Citing
Web of science 5
Scopus 5
Elibrary 5
OpenAlex 5
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