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Chromatographic and Mass Spectrometric Studies of the Features of Vanillin Desorption during Regeneration of a Highly Basic Anion Exchanger Full article

Journal Protection of Metals and Physical Chemistry of Surfaces
ISSN: 2070-2051 , E-ISSN: 2070-206X
Output data Year: 2020, Volume: 56, Number: 1, Pages: 44-48 Pages count : 5 DOI: 10.1134/s2070205119060297
Tags vanillin, highly basic anion exchanger, regeneration, side reactions, gas chromatography/mass spectrometry, matrix-activated laser desorption/ionization mass spectrometry
Authors Sholokhova A.Yu. 1 , Shashkov M.V. 2,3 , Eliseeva T.V. 4 , Buryak A.K. 1
Affiliations
1 Frumkin Institute of Physical Chemistry and Electrochemistry, Russian Academy of Sciences, Moscow, Russia
2 Boreskov Institute of Catalysis, Siberian Branch, Russian Academy of Sciences, Novosibirsk, Russia
3 Novosibirsk State University, Novosibirsk, Russia
4 Voronezh State University, Voronezh, Russia

Abstract: The occurrence of side chemical reactions during regeneration of the highly basic anion exchanger AB-17-2P with adsorbed vanillin with an alkali solution in the presence of atmospheric oxygen was confirmed by the method of gas chromatography/mass spectrometry. A number of the vanillin transformation products were identified. The method of mass spectrometry with matrix-activated laser desorption/ionization demonstrated the presence of the products of vanillin oxidation and polymerization, as well as benzoin condensation in the studied regeneration solution.
Cite: Sholokhova A.Y. , Shashkov M.V. , Eliseeva T.V. , Buryak A.K.
Chromatographic and Mass Spectrometric Studies of the Features of Vanillin Desorption during Regeneration of a Highly Basic Anion Exchanger
Protection of Metals and Physical Chemistry of Surfaces. 2020. V.56. N1. P.44-48. DOI: 10.1134/s2070205119060297 WOS Scopus РИНЦ AN OpenAlex
Original: Шолохова А.Ю. , Шашков М.В. , Елисеева Т.В. , Буряк А.К.
Хроматографическое и масс-спектрометрическое исследование особенностей процесса десорбции ванилина при регенерации высокоосновного анионообменника
Физикохимия поверхности и защита материалов. 2020. Т.56. №1. С.47-52. DOI: 10.31857/S0044185619060299 РИНЦ OpenAlex
Dates:
Submitted: Jan 29, 2019
Accepted: Feb 26, 2019
Published print: Jan 1, 2020
Published online: Apr 6, 2020
Identifiers:
Web of science: WOS:000524238900007
Scopus: 2-s2.0-85083198976
Elibrary: 43271191
Chemical Abstracts: 2020:648151
OpenAlex: W3015869570
Citing:
DB Citing
Web of science 1
Scopus 1
Elibrary 1
OpenAlex 1
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