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Transfer Hydrodechlorination of Chlorobenzene in Supercritical Isopropanol Using Monometallic and Bimetallic Catalysts Obtained by Precipitation in a Supercritical CO2 Full article

Journal The Journal of Supercritical Fluids
ISSN: 0896-8446 , E-ISSN: 1872-8162
Output data Year: 2026, Volume: 229, Article number : 106846, Pages count : DOI: 10.1016/j.supflu.2025.106846
Tags Supercritical antisolvent; Transfer hydrodechloration; Supercritical isopropanol; Chlorobenzene
Authors Romanov A.S. 1 , Nesterov N.S. 1 , Pakharukova V.P. 1 , Nasokhov D.E. 1 , Ukhterova O.A. 1 , Martyanov O.N. 1
Affiliations
1 Boreskov Institute of Catalysis SB RAS, Academician Lavrentiev ave. 5, Novosibirsk 630090, Russia

Funding (1)

1 Russian Science Foundation 24-23-20054

Abstract: Monometallic (Ni-, Co-, Cu-, and Fe-containing, Me25/Al2O3) and bimetallic (NixCo(50-x)/Al2O3) catalysts were synthesized via precipitation in supercritical carbon dioxide. The catalytic activity of these systems was evaluated in the transfer hydrodechlorination of chlorobenzene, employing supercritical isopropanol as a hydrogen donor, at temperatures ranging from 250 ◦C to 275 ◦C. The hydrodechlorination rates for monometallic catalysts followed the order: Ni25/Al2O3 > Co25/Al2O3 > Cu25/Al2O3 > > Fe25/Al2O3. For bimetallic catalysts (NixCo(50-x)/Al2O3), the hydrodechlorination rate increased with increasing nickel content. It was observed that significant coarsening of metal particle crystallites occurred during hydrodechlorination; however, this phenomenon did not demonstrably affect catalyst activity
Cite: Romanov A.S. , Nesterov N.S. , Pakharukova V.P. , Nasokhov D.E. , Ukhterova O.A. , Martyanov O.N.
Transfer Hydrodechlorination of Chlorobenzene in Supercritical Isopropanol Using Monometallic and Bimetallic Catalysts Obtained by Precipitation in a Supercritical CO2
The Journal of Supercritical Fluids. 2026. V.229. 106846 . DOI: 10.1016/j.supflu.2025.106846 WOS
Dates:
Submitted: Aug 8, 2025
Accepted: Nov 19, 2025
Published online: Nov 20, 2025
Identifiers:
Web of science: WOS:001628871200001
Citing: Пока нет цитирований
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