ICP-AES Techniques of Silicon, Germanium, and Their Oxides | Sciact - CRIS-система Института катализа

ICP-AES Techniques of Silicon, Germanium, and Their Oxides Научная публикация

Журнал

Inorganic Materials
ISSN: 0020-1685 , E-ISSN: 1608-3172

Вых. Данные

Год: 2016, Том: 52, Номер: 14, Страницы: 1431-1438 Страниц : 8 DOI: 10.1134/S0020168516140077

Ключевые слова

atomic emission spectral analysis, determination of impurities, germanium, germanium oxide (IV), inductively coupled plasma, LODs, matrix effect, silicon, silicon oxide (IV)

Авторы

Khomichenko N.N. ^1,2 , Shaverina A.V. ¹ , Tsygankova A.R. ^1,2 , Saprykin A.I. ^1,2

Организации

1	Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences, Novosibirsk, Russia
2	Novosibirsk National Research State University, Novosibirsk, Russia

The techniques of atomic emission spectrometry with inductively coupled plasma (ICP-AES) for quantitative determination impuritiesi in silicon, germanium, and their dioxides are developed. Analytical lines for siliconmatrix (29 trace elements) and germanium-matrix (42 trace elements) are selected. Matrix interferences caused by the presence of silicon and germanium in the solutions are studied. The optimal concentrations of matrix are determined. LODs for trace elements are in the range from n × 10–7 to n × 10–5 wt %; RSD < 20%. The accuracy of the results is confirmed by the method of “introduced–found.” The developed techniques are express, simple, and can determine a broad range of trace elements.

Khomichenko N.N. , Shaverina A.V. , Tsygankova A.R. , Saprykin A.I.
ICP-AES Techniques of Silicon, Germanium, and Their Oxides
Inorganic Materials. 2016. V.52. N14. P.1431-1438. DOI: 10.1134/S0020168516140077 WOS Scopus РИНЦ CAPlus OpenAlex

Хомиченко Н.Н. , Шаверина А.В. , Цыганкова А.Р. , Сапрыкин А.И.
Разработка ИСП-АЭС методик анализа кремния, германия и их оксидов
Заводская лаборатория. Диагностика материалов. 2015. Т.81. №6. С.10-15. RSCI РИНЦ

Поступила в редакцию:	24 мар. 2015 г.
Опубликована в печати:	1 дек. 2016 г.
Опубликована online:	10 февр. 2017 г.

Web of science:	WOS:000394432700007
Scopus:	2-s2.0-85011827162
РИНЦ:	29477131
Chemical Abstracts:	2017:244341
OpenAlex:	W2587398790

БД	Цитирований
Web of science	5
Scopus	4
OpenAlex	4