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Study of the Chemical and Phase Transformations in the Mechanochemical Synthesis of the MgAl-Layered Double Hydroxide Full article

Journal Journal of Alloys and Compounds
ISSN: 0925-8388 , E-ISSN: 1873-4669
Output data Year: 2022, Volume: 890, Article number : 161902, Pages count : 12 DOI: 10.1016/j.jallcom.2021.161902
Tags Layered double hydroxides; Mechanochemical activation; Structural properties
Authors Stepanova L.N. 1 , Kobzar E.O. 1 , Leont’eva N.N. 1 , Gulyaeva T.I. 1 , Vasilevich A.V. 1 , Babenko A.V. 1 , Serkova A.N. 2 , Salanov A.N. 2 , Belskaya O.B. 1
Affiliations
1 Center of New Chemical Technologies BIC, Boreskov Institute of Catalysis, Neftezavodskaya Str., 54, 644040 Omsk, Russia
2 Boreskov Institute of Catalysis, 5 Acad. Lavrentieva Ave., 630090 Novosibirsk, Russia

Funding (1)

1 Ministry of Science and Higher Education of the Russian Federation 0239-2021-0004

Abstract: Mechanochemical synthesis of MgAl-layered double hydroxides (MgAl-LDH) with molar ratio MgAl = 3 was performed. The effect of the acceleration of milling bodies (500 and 1000 m s-2), activation time (5–90 min), and water addition on the phase composition of obtained samples, their structural parameters, as well as on the process of formation of mixed oxides, prepared after LDH calcination was studied. The conditions for the preparation of single-phase LDH were established. It was shown the possibility of the textural properties regulation of mixed oxides by change of the mechanochemical synthesis parameters of corresponding layered double hydroxides.
Cite: Stepanova L.N. , Kobzar E.O. , Leont’eva N.N. , Gulyaeva T.I. , Vasilevich A.V. , Babenko A.V. , Serkova A.N. , Salanov A.N. , Belskaya O.B.
Study of the Chemical and Phase Transformations in the Mechanochemical Synthesis of the MgAl-Layered Double Hydroxide
Journal of Alloys and Compounds. 2022. V.890. 161902 :1-12. DOI: 10.1016/j.jallcom.2021.161902 WOS Scopus РИНЦ AN OpenAlex publication_identifier_short.sciact_ihcp_identifier_type
Dates:
Submitted: Jun 16, 2021
Accepted: Sep 5, 2021
Published online: Sep 8, 2021
Published print: Jan 15, 2022
Identifiers:
Web of science: WOS:000706854400003
Scopus: 2-s2.0-85114925794
Elibrary: 47102763
Chemical Abstracts: 2021:2045531
OpenAlex: W3197845296
publication_identifier.sciact_ihcp_identifier_type: 3569
Citing:
DB Citing
Scopus 18
Elibrary 13
Web of science 17
OpenAlex 18
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