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High-Resolution Diffractometer for Structural Studies of Polycrystalline Materials Full article

Journal Journal of Structural Chemistry
ISSN: 0022-4766 , E-ISSN: 1573-8779
Output data Year: 1994, Volume: 35, Number: 2, Pages: 224-228 Pages count : 5 DOI: 10.1007/BF02578312
Tags Synchrotron Radiation; Crystal Analyzer; Synchrotron Radiation Beam; Anomalous Scattering; Oscillation Curve
Authors Shmakov A.N. 1 , Mytnichenko S.V. 1 , Tsybulya S.V. 1 , Solovyeva L.P. 1 , Tolochko B.P. 1
Affiliations
1 Institute of Catalysis, Siberian Branch, Russian Academy of Sciences

Abstract: A high-resolution powder diffraction station with synchrotron radiation has been created. The diffractometer was developed on the basis of two Microcontrol precision goniometers. The latter provide the independent movement of a specimen and a detector with a minimal step of 2θ=0.001°. Using the Si(111) crystal as the analyzer, we obtained half widths of the (212), (203), and (301) reflections for α-SiO2 (0.02–0.025° 2θ). The device was tested using α-Al2O3 as the standard.
Cite: Shmakov A.N. , Mytnichenko S.V. , Tsybulya S.V. , Solovyeva L.P. , Tolochko B.P.
High-Resolution Diffractometer for Structural Studies of Polycrystalline Materials
Journal of Structural Chemistry. 1994. V.35. N2. P.224-228. DOI: 10.1007/BF02578312 WOS Scopus РИНЦ OpenAlex
Original: Шмаков А.Н. , Мытниченко С.В. , Цыбуля С.В. , Соловьева Л.П. , Толочко Б.П.
Дифрактометр высокого разрешения для структурных исследований поликристаллических материалов
Журнал структурной химии. 1994. Т.35. №2. С.85-91. РИНЦ ANCAN
Dates:
Submitted: May 13, 1993
Published print: Mar 1, 1994
Identifiers:
Web of science: WOS:A1994PR42800012
Scopus: 2-s2.0-51249164811
Elibrary: 29218981
OpenAlex: W2079989003
Citing:
DB Citing
Web of science 8
Scopus 8
Elibrary 8
OpenAlex 9
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