A Procedure of ICP-AES Analysis of Silicon Using Microwave Digestion and Preconcentration | Sciact - CRIS-system of Boreskov Institute of Catalysis

A Procedure of ICP-AES Analysis of Silicon Using Microwave Digestion and Preconcentration Full article

Journal

Journal of Analytical Chemistry
ISSN: 1061-9348 , E-ISSN: 1608-3199

Output data

Year: 2015, Volume: 70, Number: 1, Pages: 28-31 Pages count : 4 DOI: 10.1134/S1061934815010153

Tags

atomic emission spectrochemical analysis, high-purity silicon, inductively coupled plasma, limits of detection, multielemental analysis, preconcentration of impurities

Authors

Shaverina A.V. ¹ , Tsygankova A.R. ^1,2 , Saprykin A.I. ^1,2

Affiliations

1	Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences, pr. Lavrent’eva 3, Novosibirsk, 630090 Russia
2	Novosibirsk National Research State University, Pirogova 2, Novosibirsk, 630090 Russia

A combined procedure has been developed for the analysis of highpurity silicon with preliminary vaporphase digestion and preconcentration in a microwave oven using inductively coupled plasma atomic emission spectrometry (ICPAES). Liners for highpressure vessels of microwave oven ensuring the simulta neous distillation of matrices from 3–4 samples without their contact with the acid solution have been designed and manufactured. The procedure ensures the determination of up to 30 elements: Ag, Al, Be, Bi, Ca, Cd, Co, Cr, Cu, Fe, Ga, Hf, In, K, Li, Mn, Mo, Na, Nb, Ni, P, Rb, Sb, Sn, Sr, Ta, V, W, Zn, and Zr with the limits of detection 10–8 ⎯10–6 wt %.

Shaverina A.V. , Tsygankova A.R. , Saprykin A.I.
A Procedure of ICP-AES Analysis of Silicon Using Microwave Digestion and Preconcentration
Journal of Analytical Chemistry. 2015. V.70. N1. P.28-31. DOI: 10.1134/S1061934815010153 WOS Scopus РИНЦ ANCAN OpenAlex

Шаверина А.В. , Цыганкова А.Р. , Сапрыкин А.И.
Методика ИСП-АЭС анализа кремния с микроволновым разложением и концентрированием
Журнал аналитической химии. 2015. Т.70. №1. С.26-29. DOI: 10.7868/S004445021501017X РИНЦ OpenAlex

Submitted:	Oct 8, 2013
Accepted:	Dec 27, 2013
Published online:	Dec 13, 2014
Published print:	Jan 1, 2015

Web of science:	WOS:000346239700006
Scopus:	2-s2.0-85000237252
Elibrary:	24934182
Chemical Abstracts:	2014:2091153
Chemical Abstracts (print):	162:148230
OpenAlex:	W2070855488

DB	Citing
Web of science	15
Scopus	15
OpenAlex	11