Synthesis and Сharacterization of 3D Hierarchical Rutile Nanostructures: Effects of Synthesis Temperature and Reagent Concentrations on the Texture and Morphology Full article
Journal |
Nanotechnologies in Russia
ISSN: 1995-0780 , E-ISSN: 1995-0799 |
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Output data | Year: 2017, Volume: 12, Number: 3, Pages: 156-164 Pages count : 9 DOI: 10.1134/S1995078017020045 | ||||
Tags | Nanostructures; Sol-gels | ||||
Authors |
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Affiliations |
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Funding (1)
1 | Federal Agency for Scientific Organizations | 0303-2016-0004 |
Abstract:
Rutile nanostructures with a 3D hierarchical structure organization are synthesized via the sol-gel technique using TiCl4 as a titanium precursor and HCl to regulate the acidity. The effects the synthesis conditions—molar ratios of the reagents ([Cl–]/[Ti4+] and [H2O]/[Ti4+]) and temperature—have on the mechanism of formation of the rutile phase are established. We show that the texture and morphology of the rutile nanostructrures depend on the particle packing at all levels of the hierarchical organization and are directly related to the synthesis conditions.
Cite:
Bessudnova E.V.
, Shikina N.V.
, Mel’gunov M.S.
, Ismagilov Z.R.
Synthesis and Сharacterization of 3D Hierarchical Rutile Nanostructures: Effects of Synthesis Temperature and Reagent Concentrations on the Texture and Morphology
Nanotechnologies in Russia. 2017. V.12. N3. P.156-164. DOI: 10.1134/S1995078017020045 WOS Scopus РИНЦ AN OpenAlex
Synthesis and Сharacterization of 3D Hierarchical Rutile Nanostructures: Effects of Synthesis Temperature and Reagent Concentrations on the Texture and Morphology
Nanotechnologies in Russia. 2017. V.12. N3. P.156-164. DOI: 10.1134/S1995078017020045 WOS Scopus РИНЦ AN OpenAlex
Original:
Бессуднова Е.В.
, Шикина Н.В.
, Мельгунов М.С.
, Исмагилов З.Р.
Синтез и исследование 3d иерархического нанорутила. Влияние температуры синтеза и концентрации исходных компонентов на текстурные свойства и морфологию
Российские нанотехнологии. 2017. Т.12. №3-4. С.34-42. RSCI РИНЦ
Синтез и исследование 3d иерархического нанорутила. Влияние температуры синтеза и концентрации исходных компонентов на текстурные свойства и морфологию
Российские нанотехнологии. 2017. Т.12. №3-4. С.34-42. RSCI РИНЦ
Dates:
Submitted: | Aug 10, 2016 |
Accepted: | Dec 13, 2016 |
Published print: | Mar 1, 2017 |
Published online: | Apr 29, 2017 |
Identifiers:
Web of science: | WOS:000410430200005 |
Scopus: | 2-s2.0-85018274494 |
Elibrary: | 31043931 |
Chemical Abstracts: | 2017:684527 |
OpenAlex: | W2609154079 |